INDEX NAME NOT YET ASSIGNED

Base Information

• Chemical Name: INDEX NAME NOT YET ASSIGNED
• CAS No.: 893638-45-4
• Molecular Formula: C₁₃H₁₃NO₃
• Molecular Weight: 231.251
• Mol file: 893638-45-4.mol

Synonyms:5-(o-Tolyl)-isoxazole-3-carboxylic acid ethyl ester, 97%

Chemical Property of INDEX NAME NOT YET ASSIGNED

Chemical Property:

• PSA: 52.33000
• LogP: 2.82670

Purity/Quality:

5-o-Tolyl-isoxazole-3-carboxylicacidethylester 95%+ ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of INDEX NAME NOT YET ASSIGNED

There total 1 articles about INDEX NAME NOT YET ASSIGNED which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tert-butyldimethyl((1-(o-tolyl)vinyl)oxy)silane → ethyl 5-(o-tolyl)isoxazole-3-carboxylate (893638-45-4)

Guidance literature:

Multi-step reaction with 2 steps

1.1: copper(l) iodide; N,N,N',N'',N'''-pentamethyldiethylenetriamine; triethylsilyl chloride / acetonitrile / 0.08 h

1.2: 14 h / 60 °C

2.1: sodium azide / acetonitrile / 3 h / 80 °C / Schlenk technique

With copper(l) iodide; sodium azide; triethylsilyl chloride; N,N,N',N'',N'''-pentamethyldiethylenetriamine; In acetonitrile;

DOI:10.1016/j.tetlet.2021.153052

Refernces