Tetrazole-5-acetohydrazide

Base Information

• Chemical Name: Tetrazole-5-acetohydrazide
• CAS No.: 1002104-07-5
• Molecular Formula: C3H6N6O
• Molecular Weight: 142.12
• Mol file: 1002104-07-5.mol

Synonyms:Tetrazole-5-acetohydrazide

Chemical Property of Tetrazole-5-acetohydrazide

Chemical Property:

• PSA: 113.07000
• LogP: -0.72730

Purity/Quality:

97% ^*data from raw suppliers

Tetrazole-5-acetohydrazide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Tetrazole-5-acetohydrazide

There total 1 articles about Tetrazole-5-acetohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

ethyl (tetrazol-5-yl)acetate (13616-37-0) → (tetrazol-5-yl)acetic acid hydrazide (1002104-07-5)

Guidance literature:

With hydrazine hydrate; In ethanol; at 115 ℃; for 0.0833333h; Microwave irradiation;

DOI:10.1002/cmdc.201500335

Reference yield: 82.0%

(tetrazol-5-yl)acetic acid hydrazide (1002104-07-5) + 2-methylphenyl aldehyde (529-20-4) → N'-(2-methylbenzylidene)-2-(1H-tetrazol-5-yl)acetohydrazide

Guidance literature:

In methanol; at 80 ℃; for 0.0333333h; under 12751.3 Torr; Microwave irradiation;

DOI:10.1002/cmdc.201500335

Reference yield: 80.0%

(tetrazol-5-yl)acetic acid hydrazide (1002104-07-5) + o-fluorophenyl isothiocyanate (38985-64-7) → 4-(2-fluorophenyl)-1-[(tetrazol-5-yl)acetyl]thiosemicarbazide (1002104-12-2)

Guidance literature:

at 60 - 70 ℃; for 8h;

DOI:10.1016/S0385-5414(07)81198-1

upstream raw materials:

ethyl (tetrazol-5-yl)acetate

Downstream raw materials:

4-benzyl-1-[(tetrazol-5-yl)acetyl]thiosemicarbazide

4-(2-fluorophenyl)-1-[(tetrazol-5-yl)acetyl]thiosemicarbazide

4-phenyl-1-[(tetrazol-5-yl)acetyl]thiosemicarbazide

4-(4-methoxyphenyl)-1-[(tetrazol-5-yl)acetyl]thiosemicarbazide

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