2-Phenyl-8-BroMoquinoline

Base Information

• Chemical Name: 2-Phenyl-8-BroMoquinoline
• CAS No.: 871507-80-1
• Molecular Formula: C15H10BrN
• Molecular Weight: 284.155
• Hs Code.: 2933499090
• Mol file: 871507-80-1.mol

Synonyms:2-Phenyl-8-BroMoquinoline;8-Bromo-2-phenylquinoline

Chemical Property of 2-Phenyl-8-BroMoquinoline

Chemical Property:

• PSA: 12.89000
• LogP: 4.66430
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

8-Bromo-2-phenylquinoline 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-Phenyl-8-BroMoquinoline

There total 4 articles about 2-Phenyl-8-BroMoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

2,8-dibromoquinoline (871507-79-8) + phenylboronic acid (98-80-6) → 8-bromo-2-phenylquinoline (871507-80-1)

Guidance literature:

With potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; toluene; for 22h; Heating;

DOI:10.1016/j.tetlet.2005.09.120

Reference yield: 57.0%

C15H14BrN → 8-bromo-2-phenylquinoline (871507-80-1)

Guidance literature:

With oxygen; tris(p-bromophenylammoniumyl) hexachloroantimonate; In acetonitrile; at 40 ℃; for 48h;

DOI:10.1002/adsc.201500574

Reference yield: 57.0%

→ 8-bromo-2-phenylquinoline (871507-80-1)

Guidance literature:

With benzophenone; potassium tert-butylate; In 1,4-dioxane; at 90 ℃; for 1h; Inert atmosphere; Sealed tube;

upstream raw materials:

2,8-dibromoquinoline

phenylboronic acid

8-bromo-1H-quinoline-2-one

Downstream raw materials:

C₄₁H₄₀HfN₂

C₄₁H₄₀N₂Zr

N-(2,6-diisopropylphenyl)-2-phenyl-8-quinolinamine

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