N-Methyl-N-phenyl-2-vinylaniline

Base Information

Chemical Name:N-Methyl-N-phenyl-2-vinylaniline
CAS No.:1416427-14-9
Molecular Formula:C₁₅H₁₅N
Molecular Weight:209.291
Hs Code.:
Mol file:1416427-14-9.mol

Synonyms:N-Methyl-N-phenyl-2-vinylaniline

Suppliers and Price of N-Methyl-N-phenyl-2-vinylaniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of N-Methyl-N-phenyl-2-vinylaniline

Chemical Property:

Purity/Quality:: ≥99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N-Methyl-N-phenyl-2-vinylaniline

There total 5 articles about N-Methyl-N-phenyl-2-vinylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 2065-66-9
methyl-triphenylphosphonium iodide

: 208664-53-3
2-((N-methyl-N-phenyl)amino)benzaldehyde

: 1416427-14-9
2-((N-methyl-N-phenyl)amino)styrene

Guidance literature:: methyl-triphenylphosphonium iodide; With potassium tert-butylate; In tetrahydrofuran; at 0 - 20 ℃; Schlenk technique; Inert atmosphere;

2-((N-methyl-N-phenyl)amino)benzaldehyde; In tetrahydrofuran; at -60 ℃; Schlenk technique; Inert atmosphere;

Reference yield: 90.0%

: 2-(2-(tert-butyldiphenylsilyl)vinyl)-N-methyl-N-phenylaniline

: 1416427-14-9
2-((N-methyl-N-phenyl)amino)styrene

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 80 ℃; for 19h; Inert atmosphere;
DOI:10.1002/anie.201707309

Reference yield: 52.0%

: 593-60-2,25951-54-6
Vinyl bromide

: 17763-67-6
Phenyl triflate

: 100-61-8
N-methylaniline

: 1416427-14-9
2-((N-methyl-N-phenyl)amino)styrene

Guidance literature:: N-methylaniline; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.25h; Inert atmosphere; Schlenk technique; Sealed tube;

With bis(2,2,6,6-tetramethyl-1-piperidyl)zinc; In tetrahydrofuran; hexane; at -78 ℃; for 0.25h; Inert atmosphere; Schlenk technique; Sealed tube;

Vinyl bromide; Phenyl triflate; Further stages;
DOI:10.1021/acs.orglett.0c00320