1-Bromo-3-(3-bromopropyl)benzene

Base Information

Chemical Name:1-Bromo-3-(3-bromopropyl)benzene
CAS No.:109757-61-1
Molecular Formula:C9H10Br2
Molecular Weight:277.986
Hs Code.:
European Community (EC) Number:849-667-7
Nikkaji Number:J2.251.588H

Synonyms:1-BROMO-3-(3-BROMOPROPYL)BENZENE;109757-61-1;1-BROMO-3-(3-BROMOPROPYL)-BENZENE;1-Bromo-3-(3-bromo-propyl)-benzene;SCHEMBL82275;OUFNRBIRCKUZDO-UHFFFAOYSA-N;3-bromo-1-(3-bromopropyl)benzene;MFCD09744403;AKOS011898141;AB91686;CS-0376345;C77758;EN300-674452

Suppliers and Price of 1-Bromo-3-(3-bromopropyl)benzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 1-Bromo-3-(3-bromopropyl)benzene

Chemical Property:

XLogP3:4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:3
Exact Mass:277.91288
Heavy Atom Count:11
Complexity:104

Purity/Quality:: 98%min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC(=C1)Br)CCCBr

Technology Process of 1-Bromo-3-(3-bromopropyl)benzene

There total 4 articles about 1-Bromo-3-(3-bromopropyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 65537-54-4
3-(3-bromophenyl)-propan-1-ol

: 109757-61-1
1-bromo-3-(3- bromopropyl)benzene

Guidance literature:: With carbon tetrabromide; triphenylphosphine; In tetrahydrofuran; for 16h;

Reference yield:

: 3132-99-8
m-bromobenzoic aldehyde

: 109757-61-1
1-bromo-3-(3- bromopropyl)benzene

Guidance literature:: Multi-step reaction with 4 steps

1: sodium methylate / methanol / 0 - 20 °C

2: palladium 10% on activated carbon; hydrogen / 3 h / 20 °C

3: lithium aluminium tetrahydride / tetrahydrofuran / 20 °C

4: triphenylphosphine; N-Bromosuccinimide / dichloromethane / 20 °C

With N-Bromosuccinimide; lithium aluminium tetrahydride; palladium 10% on activated carbon; hydrogen; sodium methylate; triphenylphosphine; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1002/cmdc.201600343

Reference yield:

: 24398-80-9
ethyl 3-bromo-cinnamate

: 109757-61-1
1-bromo-3-(3- bromopropyl)benzene

Guidance literature:: Multi-step reaction with 3 steps

1: palladium 10% on activated carbon; hydrogen / 3 h / 20 °C

2: lithium aluminium tetrahydride / tetrahydrofuran / 20 °C

3: triphenylphosphine; N-Bromosuccinimide / dichloromethane / 20 °C

With N-Bromosuccinimide; lithium aluminium tetrahydride; palladium 10% on activated carbon; hydrogen; triphenylphosphine; In tetrahydrofuran; dichloromethane;
DOI:10.1002/cmdc.201600343