(3aR,7aR)-rel-octahydro-3a-Methyl-2H-Indol-2-one (Relative stereocheMistry)

Base Information

• Chemical Name: (3aR,7aR)-rel-octahydro-3a-Methyl-2H-Indol-2-one (Relative stereocheMistry)
• CAS No.: 82732-40-9
• Molecular Formula: C₉H₁₅NO
• Molecular Weight: 153.224

Synonyms:(3aR,7aR)-rel-octahydro-3a-Methyl-2H-Indol-2-one (Relative stereocheMistry)

Chemical Property of (3aR,7aR)-rel-octahydro-3a-Methyl-2H-Indol-2-one (Relative stereocheMistry)

Chemical Property:

• PSA: 29.10000
• LogP: 1.78400

Purity/Quality:

(3aR,7aR)-rel-octahydro-3a-methyl-2H-Indol-2-one(Relativestereochemistry) 97.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of (3aR,7aR)-rel-octahydro-3a-Methyl-2H-Indol-2-one (Relative stereocheMistry)

There total 3 articles about (3aR,7aR)-rel-octahydro-3a-Methyl-2H-Indol-2-one (Relative stereocheMistry) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

C10H17NO3S → 3a-methyl-cis-octahydroindol-2-one (82732-40-9)

Guidance literature:

With aluminum oxide; In methanol;

DOI:10.1021/jo00141a014

Reference yield:

2-Bromo-N-(2-methyl-cyclohex-2-enyl)-N-(2,2,2-trifluoro-acetyl)-acetamide → N-(2-methylcyclohex-2-en-1-yl)acetamide (83529-02-6) + 3a-methyl-cis-octahydroindol-2-one (82732-40-9)

Guidance literature:

With potassium fluoride; tin hydride; Yield given. Multistep reaction. Yields of byproduct given;

DOI:10.3987/COM-88-S137

Reference yield:

2-Bromo-N-(2-methyl-cyclohex-2-enyl)-acetamide (124706-19-0) → 3a-methyl-cis-octahydroindol-2-one (82732-40-9)

Guidance literature:

Multi-step reaction with 2 steps

1: poly (4-vinylpyridine)

2: 1.) Ph₃GeH, AlBN, 2.) aqueous potassium fluoride / 1.) benzene, 80 deg C

With potassium fluoride; 2,2'-azobis(isobutyronitrile); poly (4-vinylpyridine); triphenylgermane;

DOI:10.3987/COM-88-S137

upstream raw materials:

2-Bromo-N-(2-methyl-cyclohex-2-enyl)-acetamide

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