2-Methyl-2-propanyl isopropyl(2-oxoethyl)carbamate

Base Information

Chemical Name:2-Methyl-2-propanyl isopropyl(2-oxoethyl)carbamate
CAS No.:844851-97-4
Molecular Formula:C10H19NO3
Molecular Weight:201.266
Hs Code.:

Synonyms:tert-butyl isopropyl(2-oxoethyl)carbaMate

Suppliers and Price of 2-Methyl-2-propanyl isopropyl(2-oxoethyl)carbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 2-Methyl-2-propanyl isopropyl(2-oxoethyl)carbamate

Chemical Property:

Purity/Quality:: 99% ，98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-Methyl-2-propanyl isopropyl(2-oxoethyl)carbamate

There total 5 articles about 2-Methyl-2-propanyl isopropyl(2-oxoethyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.82%

: 610309-73-4
tert-butyl N-(2-hydroxyethyl)-N-(propan-2-yl)carbamate

: 844851-97-4
1,1-dimethylethyl (1-methylethyl)(2-oxoethyl)carbamate

Guidance literature:: With Dess-Martin periodane; In dichloromethane; at 20 ℃; for 2h;

Reference yield:

: isopropyl-(3-methyl-but-2-enyl)-carbamic acid tert-butyl ester

: 844851-97-4
1,1-dimethylethyl (1-methylethyl)(2-oxoethyl)carbamate

Guidance literature:: With ozone; In methanol; dichloromethane; at -78 ℃; for 0.5h;
DOI:10.1002/hlca.200690157

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 844851-97-4
1,1-dimethylethyl (1-methylethyl)(2-oxoethyl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / DMAP / tetrahydrofuran / 19 h / 20 °C

2: KH / dimethylformamide / 3.5 h / 0 - 25 °C

3: 1.790 g / O₃ / methanol; CH₂Cl₂ / 0.5 h / -78 °C

With dmap; potassium hydride; ozone; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/hlca.200690157