ETHYL 6-ACETYLNICOTINATE

Base Information

Chemical Name:ETHYL 6-ACETYLNICOTINATE
CAS No.:20857-24-3
Molecular Formula:C₁₀H₁₁NO₃
Molecular Weight:193.202
Hs Code.:2933399090
Mol file:20857-24-3.mol

Synonyms:ETHYL 6-ACETYLNICOTINATE

Suppliers and Price of ETHYL 6-ACETYLNICOTINATE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
Ethyl6-acetylnicotinate 95+%
1g
$ 825.00

Chemenu
ethyl6-acetylnicotinate 95%
1g
$ 779.00

Alichem
Ethyl6-acetylnicotinate
100g
$ 8238.32

Alichem
Ethyl6-acetylnicotinate
25g
$ 2898.42

Alichem
Ethyl6-acetylnicotinate
10g
$ 1704.48

Total 5 raw suppliers

Chemical Property of ETHYL 6-ACETYLNICOTINATE

Chemical Property:

PSA：56.26000
LogP:1.46090
Storage Temp.:2-8°C

Purity/Quality:

98%min ^*data from raw suppliers

Ethyl6-acetylnicotinate 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of ETHYL 6-ACETYLNICOTINATE

There total 2 articles about ETHYL 6-ACETYLNICOTINATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 19.0%

: 614-18-6
3-pyridinecarboxylic acid ethyl ester

: 75-07-0,9002-91-9
acetaldehyde

: 36046-36-3
2,4-Diacetyl-nicotinsaeureethylester

: 20857-24-3
6-acetyl-nicotinic acid ethyl ester

: 4-Acetyl-nicotinic acid ethyl ester

Guidance literature:: With tert.-butylhydroperoxide; sulfuric acid; iron(II) sulfate; at 5 - 10 ℃; Yield given;
DOI:10.1055/s-1998-2046

Reference yield:

: 20857-24-3
6-acetyl-nicotinic acid ethyl ester

Guidance literature:

Reference yield:

: 20857-24-3
6-acetyl-nicotinic acid ethyl ester

: 153559-73-0
ethyl 6-(1-(3,5,5,8,8-pentamethyl-5,6,7,8-tetrahydronaphthalen-2-yl)vinyl)nicotinate

Guidance literature:: Multi-step reaction with 3 steps

1: hydrazine hydrate / ethanol / 1 h / Reflux

2: [bis(acetoxy)iodo]benzene / dichloromethane / 0.5 h / 20 °C

3: (bis(tricyclohexyl)phosphine)palladium(II) dichloride; potassium carbonate; nickel(II) acetate tetrahydrate / toluene / 24 h / 130 °C / Inert atmosphere; Sealed tube

With (bis(tricyclohexyl)phosphine)palladium(II) dichloride; [bis(acetoxy)iodo]benzene; nickel(II) acetate tetrahydrate; potassium carbonate; hydrazine hydrate; In ethanol; dichloromethane; toluene;
DOI:10.1002/adsc.201500967