3-Furancarboxylicacid,4,5-dihydro-2-methyl-5-methylene-,methylester(9CI)

Base Information

Chemical Name:3-Furancarboxylicacid,4,5-dihydro-2-methyl-5-methylene-,methylester(9CI)
CAS No.:146896-48-2
Molecular Formula:C8H10O3
Molecular Weight:154.166
Hs Code.:
Mol file:146896-48-2.mol

Synonyms:3-Furancarboxylicacid,4,5-dihydro-2-methyl-5-methylene-,methylester(9CI)

Suppliers and Price of 3-Furancarboxylicacid,4,5-dihydro-2-methyl-5-methylene-,methylester(9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 2 raw suppliers

Chemical Property of 3-Furancarboxylicacid,4,5-dihydro-2-methyl-5-methylene-,methylester(9CI)

Chemical Property:

PSA：35.53000
LogP:1.36740

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

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Technology Process of 3-Furancarboxylicacid,4,5-dihydro-2-methyl-5-methylene-,methylester(9CI)

There total 1 articles about 3-Furancarboxylicacid,4,5-dihydro-2-methyl-5-methylene-,methylester(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 101413-11-0
methyl 2-acetylpent-4-ynoate

: 6148-34-1
methyl 2,5-dimethylfuran-3-carboxylate

: 146896-48-2
methyl 2-methyl-5-methylene-4,5-dihydrofuran-3-carboxylate

Guidance literature:: With tungsten hexacarbonyl; triethylamine; In toluene; for 18h; Irradiation; Inert atmosphere;
DOI:10.1055/s-0032-1316536

Reference yield: 87.0%

: 4393-06-0
1-Phenyl-2-propen-1-ol

: 146896-48-2
methyl 2-methyl-5-methylene-4,5-dihydrofuran-3-carboxylate

: C₁₇H₁₈O₃

Guidance literature:: With iron(II) triflate; (S)-(+)-N-(3,5-dioxa-4-phosphacyclohepta-[2,1-a;3,4-a′]dinaphthalen-4-yl)dibenz[b,f]azepine; bis(1,5-cyclooctadiene)diiridium(I) dichloride; In 1,2-dichloro-ethane; at 20 ℃; for 36h; enantioselective reaction; Schlenk technique; Molecular sieve; Inert atmosphere;
DOI:10.1002/anie.201904156

Reference yield: 87.0%

: 146896-48-2
methyl 2-methyl-5-methylene-4,5-dihydrofuran-3-carboxylate

: 170938-13-3
α-vinyl-(4-phenyl-phenyl)methanol

: C₂₃H₂₂O₃

Guidance literature:: With iron(II) triflate; (S)-(+)-N-(3,5-dioxa-4-phosphacyclohepta-[2,1-a;3,4-a′]dinaphthalen-4-yl)dibenz[b,f]azepine; bis(1,5-cyclooctadiene)diiridium(I) dichloride; In 1,2-dichloro-ethane; at 20 ℃; for 36h; enantioselective reaction; Schlenk technique; Molecular sieve; Inert atmosphere;
DOI:10.1002/anie.201904156