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Technology Process of 4-Epiminocycline

4-Epiminocycline

Base Information
  • Chemical Name:4-Epiminocycline
  • CAS No.:43168-51-0
  • Molecular Formula:C23H27N3O7
  • Molecular Weight:457.483
  • Hs Code.:
  • Mol file:43168-51-0.mol
4-Epiminocycline

Synonyms:4-Epiminocycline;[4R-(4a,4ab,5ab,12ab)]-4,7-Bis(dimethylamino)-1,4,4a,5,5a,6,11,12a-octahydro-3,10,12,12a-tetrahydro-1,11-dioxo-2-naphthacenecarboxamide;Epiminocycline;[4R-(4a,4a,5a,12a)]-4,7-Bis(dimethylamino)-1,4,4a,5,5a,6,11,12a-octahydro-3,10,12,12a-tetrahydro-1,11-dioxo-2-naphthacenecarboxamide;4-Epi Minocycline (approximately 60% pure, contains unidentified salts);4-Epi Minocycline (>80%, contains unidentified salts);[4R-(4α,4aβ,5aβ,12aβ)]-4,7-Bis(diMethylaMino)-1,4,4a,5,5a,6,11,12a-octahydro-3,10,12,12a-tetrahydro-1,11-dioxo-2-naphthacenecarboxaMide;Minocycline EP IMpurity A

Suppliers and Price of 4-Epiminocycline
Supply Marketing:
Business phase:
The product has achieved commercial mass production*data from LookChem market partment
Manufacturers and distributors:
  • Manufacture/Brand
  • Chemicals and raw materials
  • Packaging
  • price
  • Usbiological
  • 4-Epiminocycline
  • 1mg
  • $ 602.00
  • TRC
  • 4-EpiMinocycline(>80%,containsunidentifiedsalts)
  • 1mg
  • $ 295.00
  • Cayman Chemical
  • 4-epi Minocycline
  • 500μg
  • $ 460.00
  • American Custom Chemicals Corporation
  • 4-EPI MINOCYCLINE 90.00%
  • 5MG
  • $ 2887.50
  • American Custom Chemicals Corporation
  • 4-EPI MINOCYCLINE 90.00%
  • 1MG
  • $ 979.85
Total 16 raw suppliers
Chemical Property of 4-Epiminocycline
Chemical Property:
  • Melting Point:>196°C (dec) 
  • PSA：164.63000 
  • LogP:0.88690 
  • Storage Temp.:Amber Vial, -20°C Freezer, Under Inert Atmosphere 
  • Solubility.:Aquepus Acid (Slightly), DMSO (Slightly), Methanol (Slightly) 
Purity/Quality:

99%, *data from raw suppliers

4-Epiminocycline *data from reagent suppliers

Safty Information:
  • Pictogram(s):  
  • Hazard Codes: 
MSDS Files:

SDS file from LookChem

Useful:
  • Uses 4-Epi Minocycline (Minocycline EP Impurity A) is an impurity of Minocycline.
Technology Process of 4-Epiminocycline

There total 2 articles about 4-Epiminocycline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

minocycline
10118-90-8,43168-51-0

minocycline

Guidance literature:
9-tert.Butyl-tetracyclinverb.V, CF3SO3H, Anisol (regioselektiv);

Reference yield:

minocycline
10118-90-8,43168-51-0

minocycline

Guidance literature:
7-Nitro-6-demethyl-6-desoxy-tetracyclin-monosulfat, 2-Methoxy-ethanol, 40percentig. wss. CH2O, H2, Pd/C, wss. n-H2SO4;
DOI:10.1021/jm00313a009
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