Methyl 3,6-anhydro-α-D-galactopyranoside

Base Information

Chemical Name:Methyl 3,6-anhydro-α-D-galactopyranoside
CAS No.:5540-31-8
Molecular Formula:C7H12O5
Molecular Weight:176.169
Hs Code.:2932999099
Mol file:5540-31-8.mol

Synonyms:1-O-Methyl-3,6-anhydro-α-D-galactopyranose;Methyl 3,6-anhydro-α-D-galactopyranoside;Methyl 3,6-anhydro-α-D-galactose;Methyl 3,6-anhydro-alpha-D-galactopyranosid;Methyl 3,6-anhydro-alpha-D-galactoside

Suppliers and Price of Methyl 3,6-anhydro-α-D-galactopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Biosynth Carbosynth
Methyl 3,6-anhydro-a-D-galactopyranoside
100 mg
$ 250.00

Biosynth Carbosynth
Methyl 3,6-anhydro-a-D-galactopyranoside
50 mg
$ 160.00

Biosynth Carbosynth
Methyl 3,6-anhydro-a-D-galactopyranoside
25 mg
$ 85.00

AK Scientific
Methyl3,6-anhydro-alpha-d-galactopyranoside
100mg
$ 387.00

AK Scientific
Methyl3,6-anhydro-alpha-d-galactopyranoside
50mg
$ 266.00

Total 4 raw suppliers

Chemical Property of Methyl 3,6-anhydro-α-D-galactopyranoside

Chemical Property:

PSA：68.15000
LogP:-1.52170
Storage Temp.:?20°C

Purity/Quality:

95% ^*data from raw suppliers

Methyl 3,6-anhydro-a-D-galactopyranoside ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Methyl 3,6-anhydro-α-D-galactopyranoside

There total 1 articles about Methyl 3,6-anhydro-α-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7732-18-5
water

: 345892-40-2
methyl-(O⁶-sulfo-α-D-mannopyranoside)

: 3056-46-0,5540-31-8,13407-60-8,15814-56-9,73977-55-6,85081-03-4,110115-41-8
methyl-(3,6-anhydro-α-D-mannopyranoside)

: 617-04-9
(2R,3S,4S,5S,6S)-2-(hydroxymethyl)-6-methoxytetrahydro-2H-pyran-3,4,5-triol

Guidance literature:: DOI:10.1039/jr9410000830

Reference yield:

: 5540-31-8
methyl 3,6-anhydro-α-D-galactopyranoside

: 31880-44-1,50611-36-4,53905-78-5,62860-21-3,67335-85-7,133907-42-3,133907-44-5,134054-60-7
tetra-O-acetyl-L-1,4-anhydro-galactitol

Guidance literature:: Multi-step reaction with 2 steps

1: aqueous sulfuric acid / Behandeln der mit wss. Natronlauge neutralisierten Reaktionsloesung mit Natrium-Amalgam unter Einleiten von Kohlendioxid

2: pyridine

With pyridine; sulfuric acid;
DOI:10.1021/ja01210a004

Reference yield:

: 5540-31-8
methyl 3,6-anhydro-α-D-galactopyranoside

: 132895-15-9
methyl 3,6-anhydro-4-O-(2,3,6-tri-O-acetyl-4-O-benzyl-β-D-galactopyranosyl)-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 1) barium oxide, barium hydroxide hydrate / 1) DMF, 0 deg C, 30 min, 2) DMF, 4 deg C, 48 h

2: 68 percent / mercury cyanide, 4 Angstroem molecular sieve / benzene / 60 °C

3: 27 percent / H₂ / 10percent Pd-C / ethyl acetate / 760 Torr

With barium hydroxide monohydrate; 4 A molecular sieve; hydrogen; mercury(II) cyanide; barium(II) oxide; palladium on activated charcoal; In ethyl acetate; benzene;
DOI:10.1016/0008-6215(90)80087-J