2,6-Bis(benzyloxy)-3-bromopyridine

Base Information

• Chemical Name: 2,6-Bis(benzyloxy)-3-bromopyridine
• CAS No.: 16727-47-2
• Molecular Formula: C19H16BrNO2
• Molecular Weight: 370.246
• Hs Code.: 2933399090
• Mol file: 16727-47-2.mol

Synonyms:2,6-Bis(benzyloxy)-3-bromopyridine

Chemical Property of 2,6-Bis(benzyloxy)-3-bromopyridine

Chemical Property:

• Boiling Point: 455.4±40.0 °C(Predicted)
• PKA: 0.22±0.34(Predicted)
• PSA: 31.35000
• Density: 1.380±0.06 g/cm3(Predicted)
• LogP: 5.00210
• Storage Temp.: Room temperature.

Purity/Quality:

97% ^*data from raw suppliers

2,6-Bis(benzyloxy)-3-bromopyridine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 2,6-Bis(benzyloxy)-3-bromopyridine was a useful reagent in the study of bacterial oxidation of nicotine.

Technology Process of 2,6-Bis(benzyloxy)-3-bromopyridine

There total 5 articles about 2,6-Bis(benzyloxy)-3-bromopyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

2,6-bis(benzyloxy)pyridine (16727-46-1) → 2,6-bis(benzyloxy)-3-bromopyridine (16727-47-2)

Guidance literature:

With N-Bromosuccinimide; In acetonitrile; at 80 ℃; for 2h;

Reference yield: 78.0%

3-bromo-2,6-difluoro-pyridine (80392-79-6) + benzyl alcohol (100-51-6,185532-71-2) → 2,6-bis(benzyloxy)-3-bromopyridine (16727-47-2)

Guidance literature:

With caesium carbonate; In acetonitrile; at 100 ℃; for 16h;

Reference yield: 78.0%

3-bromo-2,6-difluoro-pyridine (80392-79-6) → 2,6-bis(benzyloxy)-3-bromopyridine (16727-47-2)

Guidance literature:

With caesium carbonate; benzyl alcohol; In Petroleum ether;

upstream raw materials:

2,6-bis(benzyloxy)pyridine

benzyl alcohol

2,6-dichloropyridine

3-bromo-2,6-difluoro-pyridine

Downstream raw materials:

(1R)-D-O²,O⁴;O³,O⁵-(R,R)-dibenzylidene-1-(2,6-bis-benzyloxy-pyridin-3-yl)-ribitol

(1S)-D-O²,O⁴;O³,O⁵-(R,R)-dibenzylidene-1-(2,6-bis-benzyloxy-pyridin-3-yl)-ribitol

1-(2,6-bis-benzyloxy-pyridin-3-yl)-ξ-D-erythro-1,2-dideoxy-pentofuranose

5,5'-di-β-D-ribopyranosyl-3H,3'H-3,3'-azanylylidene-bis-pyridine-2,6-dione

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