3,5-diallyl-2-hydroxy-benzaldehyde

Base Information

• Chemical Name: 3,5-diallyl-2-hydroxy-benzaldehyde
• CAS No.: 159968-52-2
• Molecular Formula: C₁₃H₁₄O₂
• Molecular Weight: 202.253

Synonyms:4-sulfamido-benzyl-1,4-diazacycloheptane;4-(1,4-diazepan-1-ylmethyl)benzenesulfonamide;-(1,4-diazepan-1-ylmethyl)benzenesulfonamide

Chemical Property of 3,5-diallyl-2-hydroxy-benzaldehyde

Chemical Property:

• Vapor Pressure: 0.000703mmHg at 25°C
• Boiling Point: 298.7°C at 760 mmHg
• Flash Point: 126°C
• Density: 1.073g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3,5-diallyl-2-hydroxy-benzaldehyde

There total 3 articles about 3,5-diallyl-2-hydroxy-benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

3-allyl-2-(allyloxy)benzaldehyde (84682-15-5) → 3,5-diallylsalicylaldehyde (159968-52-2)

Guidance literature:

for 0.166667h; Neat (no solvent); Microwave irradiation;

Reference yield: 40.0%

3-allylsalicylaldehyde (24019-66-7) + allyl bromide (106-95-6) → 3,5-diallylsalicylaldehyde (159968-52-2)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 3h;

DOI:10.1021/jm900722z

Reference yield:

3-allyl-2-(allyloxy)benzaldehyde (84682-15-5) → 2,6-diallylphenol (3382-99-8) + 3,5-diallylsalicylaldehyde (159968-52-2)

Guidance literature:

upstream raw materials:

3-allyl-2-(allyloxy)benzaldehyde

3-allylsalicylaldehyde

allyl bromide

Downstream raw materials:

2-(4-benzylpiperazin-1-yl)-N'-(3,5-diallyl-2-hydroxybenzylidene)acetohydrazide

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