2-AMINO-N-ETHYLBENZENESULFONAMIDE

Base Information

• Chemical Name: 2-AMINO-N-ETHYLBENZENESULFONAMIDE
• CAS No.: 98489-77-1
• Molecular Formula: C8H12N2O2S
• Molecular Weight: 200.261
• Hs Code.: 2935009090
• Mol file: 98489-77-1.mol

Synonyms:2-AMINO-N-ETHYLBENZENESULFONAMIDE

Chemical Property of 2-AMINO-N-ETHYLBENZENESULFONAMIDE

Chemical Property:

• PSA: 80.57000
• LogP: 2.61990
• Storage Temp.: Keep in dark place,Sealed in dry,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

2-Amino-N-ethylbenzenesulfonamide 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-AMINO-N-ETHYLBENZENESULFONAMIDE

There total 3 articles about 2-AMINO-N-ETHYLBENZENESULFONAMIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

N-Ethyl-2-nitrobenzenesulfonamide (23530-41-8) → 2-amino-N-ethylbenzene-1-sulfonamide (98489-77-1)

Guidance literature:

With tin(II) chloride dihdyrate; In ethyl acetate; for 18h; Reflux;

DOI:10.1039/d1ob00968k

Reference yield:

2-Nitrobenzenesulfonyl chloride (1694-92-4) → 2-amino-N-ethylbenzene-1-sulfonamide (98489-77-1)

Guidance literature:

Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 12 h / 0 - 20 °C

2: zinc; ammonium chloride / methanol / 0 - 20 °C / Inert atmosphere

With ammonium chloride; triethylamine; zinc; In methanol; dichloromethane;

DOI:10.1039/d1cc00793a

Reference yield:

→ 2-amino-N-ethylbenzene-1-sulfonamide (98489-77-1)

Guidance literature:

upstream raw materials:

N-Ethyl-2-nitrobenzenesulfonamide

2-Nitrobenzenesulfonyl chloride

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