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6Abeta-aporphine-10,11-diol, hydrochloride (8ci)

Base Information
  • Chemical Name:6Abeta-aporphine-10,11-diol, hydrochloride (8ci)
  • CAS No.:5896-07-1
  • Molecular Formula:C17H18ClNO2
  • Molecular Weight:303.78332
  • Hs Code.:
  • Mol file:5896-07-1.mol
6Abeta-aporphine-10,11-diol, hydrochloride (8ci)

Synonyms:4H-Dibenzo(de,G)quinoline-10,11-diol, 5,6,6A,7-tetrahydro-6-methyl-, hydrochloride (1:1), (6ar)-;5,6,6A,7-Tetrahydro-6-methyl-4H-dibenzo(de,G)chinolin-10,11-diol hydrochlorid;6Abeta-aporphine-10,11-diol, hydrochloride (8ci);6A-beta-Noraporphine-10,11-diol, 6-methyl-, hydrochloride

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Chemical Property of 6Abeta-aporphine-10,11-diol, hydrochloride (8ci)
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Technology Process of 6Abeta-aporphine-10,11-diol, hydrochloride (8ci)

There total 27 articles about 6Abeta-aporphine-10,11-diol, hydrochloride (8ci) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With hydrogenchloride; calcium chloride; In water; at 45 - 145 ℃; for 2h; Inert atmosphere;
Guidance literature:
Multi-step reaction with 4 steps
1: 95 percent
2: 85 percent / pyridine / 1.) 0 deg C, 2 h, 2.) r.t., 24 h
3: 80 percent / tetrabutylammonium fluoride / acetonitrile / 3 h / Heating
4: 1.) methanesulfonic acid, 2.) hydrochloric acid / 1.) 100 deg C, 30 min, 2.) ethanol
With pyridine; hydrogenchloride; methanesulfonic acid; tetrabutyl ammonium fluoride; In acetonitrile;
Guidance literature:
Multi-step reaction with 3 steps
1: 85 percent / pyridine / 1.) 0 deg C, 2 h, 2.) r.t., 24 h
2: 80 percent / tetrabutylammonium fluoride / acetonitrile / 3 h / Heating
3: 1.) methanesulfonic acid, 2.) hydrochloric acid / 1.) 100 deg C, 30 min, 2.) ethanol
With pyridine; hydrogenchloride; methanesulfonic acid; tetrabutyl ammonium fluoride; In acetonitrile;
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