5-Phenyl-5,10-dihydroacridophosphine

Base Information

• Chemical Name: 5-Phenyl-5,10-dihydroacridophosphine
• CAS No.: 59273-35-7
• Molecular Formula: C19H15P
• Molecular Weight: 274.3
• DSSTox Substance ID: DTXSID801291632
• Nikkaji Number: J90.035D
• Mol file: 59273-35-7.mol

Synonyms:5,10-Dihydro-5-phenylacridophosphine;59273-35-7;5-phenyl-10H-acridophosphine;5-Phenyl-5,10-dihydroacridophosphine;DTXSID801291632;5-Phenyl-5,10-dihydroacridophosphine #;9,10-Dihydro-9-phenyl-9-phosphaanthracene

Chemical Property of 5-Phenyl-5,10-dihydroacridophosphine

Chemical Property:

• Boiling Point: 140 °C (0.01 mmHg)
• PSA: 13.59000
• LogP: 3.34900
• XLogP3: 4.6
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 1
• Exact Mass: 274.091137476
• Heavy Atom Count: 20
• Complexity: 298

Purity/Quality:

98%,99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1C2=CC=CC=C2P(C3=CC=CC=C31)C4=CC=CC=C4

Technology Process of 5-Phenyl-5,10-dihydroacridophosphine

There total 2 articles about 5-Phenyl-5,10-dihydroacridophosphine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

5,10-dihydro-10-phenyldibenzophosphorine-5-one (54086-39-4) → 9-phenyl-9,10-dihydro-9-phosphaanthracene (59273-35-7)

Guidance literature:

With lithium aluminium tetrahydride; aluminium trichloride; In diethyl ether; for 1h; Ambient temperature;

DOI:10.1021/jo00233a030

Reference yield:

phenylmagnesium bromide + 5-chloro-5,10-dihydro-acridophosphine (15309-64-5) → 9-phenyl-9,10-dihydro-9-phosphaanthracene (59273-35-7)

Guidance literature:

DOI:10.1016/0040-4020(76)80031-2

Reference yield: 63.0%

9-phenyl-9,10-dihydro-9-phosphaanthracene (59273-35-7) → 10-Phenyl-9,10-dihydro-10-λ5-acridophosphin-9,10-dion (54086-38-3) + 9-phenyl-9,10-dihydro-9-phosphaanthracene 9-oxide (59590-82-8)

Guidance literature:

With dihydrogen peroxide; In acetone; at 0 ℃; for 0.5h;

DOI:10.1021/jo00233a030

upstream raw materials:

5-chloro-5,10-dihydro-acridophosphine

5,10-dihydro-10-phenyldibenzophosphorine-5-one

Downstream raw materials:

5-benzyl-5-phenyl-5,10-dihydro-acridophosphinium; bromide

10-Phenyl-9,10-dihydro-10-λ⁵-acridophosphin-9,10-dion

9-phenyl-9,10-dihydro-9-phosphaanthracene 9-oxide

5-benzyl-5-phenyl-5λ⁵-acridophosphine

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