(6S,8S,9S)-8-azido-7,8,9,10-tetrahydro-2H,6H-6,9-epoxypyrimido[2,1-b][1,3]oxazocin-2-one

Base Information

Chemical Name:(6S,8S,9S)-8-azido-7,8,9,10-tetrahydro-2H,6H-6,9-epoxypyrimido[2,1-b][1,3]oxazocin-2-one
CAS No.:120826-45-1
Molecular Formula:C₉H₉N₅O₃
Molecular Weight:235.202
Hs Code.:

Synonyms:6,9-Epoxy-2H,6H-pyrimido[2,1-b][1,3]oxazocin-2-one,8-azido-7,8,9,10-tetrahydro-, [6R-(6a,8a,9a)]-;2,5'-Anhydro-3'-azido-2',3'-dideoxyuridine

Suppliers and Price of (6S,8S,9S)-8-azido-7,8,9,10-tetrahydro-2H,6H-6,9-epoxypyrimido[2,1-b][1,3]oxazocin-2-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of (6S,8S,9S)-8-azido-7,8,9,10-tetrahydro-2H,6H-6,9-epoxypyrimido[2,1-b][1,3]oxazocin-2-one

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
Density:g/cm³

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (6S,8S,9S)-8-azido-7,8,9,10-tetrahydro-2H,6H-6,9-epoxypyrimido[2,1-b][1,3]oxazocin-2-one

There total 3 articles about (6S,8S,9S)-8-azido-7,8,9,10-tetrahydro-2H,6H-6,9-epoxypyrimido[2,1-b][1,3]oxazocin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 100898-89-3
3'-azido-5'-O-(p-tolylsulfonyl)-2',3'-dideoxyuridine

: 120826-45-1
2,5'-anhydro-3'-azido-2',3'-dideoxyuridine

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile; for 1h; Heating;
DOI:10.1021/jm00128a034

Reference yield: 67.0%

: 120966-80-5
3'-azido-5'-iodo-2',3',5'-trideoxyuridine

: 120826-45-1
2,5'-anhydro-3'-azido-2',3'-dideoxyuridine

Guidance literature:: With silver(I) acetate; In acetonitrile; for 1h; Heating;
DOI:10.1021/jm00128a034

Reference yield:

: 84472-85-5
Navuridine

: 120826-45-1
2,5'-anhydro-3'-azido-2',3'-dideoxyuridine

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / pyridine / 4 °C

2: 67 percent / DBU / acetonitrile / 1 h / Heating

With pyridine; 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile;
DOI:10.1021/jm00128a034