2-Acetyl-3,5,8-trihydroxy-6-methoxy-1,4-naphthalenedione

Base Information

Chemical Name:2-Acetyl-3,5,8-trihydroxy-6-methoxy-1,4-naphthalenedione
CAS No.:15254-72-5
Molecular Formula:C₁₃H₁₀O₇
Molecular Weight:278.218
Hs Code.:2914690090
Mol file:15254-72-5.mol

Synonyms:2-Acetyl-3,5,8-trihydroxy-6-methoxy-1,4-naphthalenedione;2-Acetyl-3,5,8-trihydroxy-6-methoxy-1,4-naphthoquinone;3-Acetyl-2-hydroxy-7-methoxynaphthazarin

Suppliers and Price of 2-Acetyl-3,5,8-trihydroxy-6-methoxy-1,4-naphthalenedione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 2-Acetyl-3,5,8-trihydroxy-6-methoxy-1,4-naphthalenedione

Chemical Property:

PSA：121.13000
LogP:0.91530

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-Acetyl-3,5,8-trihydroxy-6-methoxy-1,4-naphthalenedione

There total 5 articles about 2-Acetyl-3,5,8-trihydroxy-6-methoxy-1,4-naphthalenedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 83571-28-2
6-acetyl-5,8-diacetoxy-2,7-dimethoxy-1,4-naphthoquinone

: 15254-72-5
3-acetyl-7-methoxy-2,5,8-trihydroxy-1,4-naphthoquinone

Guidance literature:: With hydrogenchloride; for 0.166667h; Heating;
DOI:10.1016/0040-4020(82)80244-5

Reference yield:

: 2644-68-0
2,5,7,8-tetramethoxy-1,4-naphthoquinone

: 15254-72-5
3-acetyl-7-methoxy-2,5,8-trihydroxy-1,4-naphthoquinone

Guidance literature:: Multi-step reaction with 5 steps

1: 65 percent / Zn, NaOAc / 1 h / Heating

2: 60 percent / ethanol; glycerol / 12 h / Irradiation

3: 80 percent / NaOAc / 1 h / Heating

4: AgO, HNO₃aq / dioxane / 0.17 h / Ambient temperature

5: 70 percent / HClaq / 0.17 h / Heating

With hydrogenchloride; silver(II) oxide; nitric acid; sodium acetate; zinc; In 1,4-dioxane; ethanol; glycerol;
DOI:10.1016/0040-4020(82)80244-5

Reference yield:

: 83571-26-0
2-acetyl-4-acetoxy-3,5,6,8-tetramethoxy-1-naphthol

: 15254-72-5
3-acetyl-7-methoxy-2,5,8-trihydroxy-1,4-naphthoquinone

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / NaOAc / 1 h / Heating

2: AgO, HNO₃aq / dioxane / 0.17 h / Ambient temperature

3: 70 percent / HClaq / 0.17 h / Heating

With hydrogenchloride; silver(II) oxide; nitric acid; sodium acetate; In 1,4-dioxane;
DOI:10.1016/0040-4020(82)80244-5