5-AMINO-1-METHYL-2-(METHYLTHIO)-1H-IMIDAZOLE-4-CARBOXAMIDE

Base Information

• Chemical Name: 5-AMINO-1-METHYL-2-(METHYLTHIO)-1H-IMIDAZOLE-4-CARBOXAMIDE
• CAS No.: 52868-68-5
• Molecular Formula: C₆H₁₀N₄OS
• Molecular Weight: 186.238
• Hs Code.: 2934999090
• Mol file: 52868-68-5.mol

Synonyms:5-AMINO-1-METHYL-2-(METHYLTHIO)-1H-IMIDAZOLE-4-CARBOXAMIDE;5-amino-1-methyl-2-(methylthio)-1H-imidazole-4-carboxamide(SALTDATA: FREE)

Chemical Property of 5-AMINO-1-METHYL-2-(METHYLTHIO)-1H-IMIDAZOLE-4-CARBOXAMIDE

Chemical Property:

• Vapor Pressure: 3.75E-08mmHg at 25°C
• Boiling Point: 446.1°C at 760 mmHg
• Flash Point: 223.6°C
• PSA: 112.23000
• Density: 1.55g/cm³
• LogP: 1.10460

Purity/Quality:

97% ^*data from raw suppliers

5-amino-1-methyl-2-(methylthio)-1H-imidazole-4-carboxamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5-AMINO-1-METHYL-2-(METHYLTHIO)-1H-IMIDAZOLE-4-CARBOXAMIDE

There total 1 articles about 5-AMINO-1-METHYL-2-(METHYLTHIO)-1H-IMIDAZOLE-4-CARBOXAMIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-amino-1-methyl-2-thioxo-2,3-dihydro-1H-imidazole-4-carboxylic acid amide (52868-67-4) + dimethyl sulfate (77-78-1) → 5-amino-1-methyl-2-methylsulfanyl-1H-imidazole-4-carboxylic acid amide (52868-68-5)

Guidance literature:

With sodium hydroxide; water;

DOI:10.1039/jr9490002329

Reference yield:

5-amino-1-methyl-2-methylsulfanyl-1H-imidazole-4-carboxylic acid amide (52868-68-5) → 9-Methyl-8-methylthioxanthin (40848-30-4)

Guidance literature:

Multi-step reaction with 2 steps

1: acetone

2: pyridine

With pyridine; acetone;

DOI:10.1039/jr9490002329

Reference yield:

5-amino-1-methyl-2-methylsulfanyl-1H-imidazole-4-carboxylic acid amide (52868-68-5) + phenyl chlorothioformate (13464-19-2) → (5-carbamoyl-3-methyl-2-methylsulfanyl-3H-imidazol-4-yl)-carbothioamidoic acid S-phenyl ester

Guidance literature:

With acetone;

DOI:10.1039/jr9490002329

upstream raw materials:

5-amino-1-methyl-2-thioxo-2,3-dihydro-1H-imidazole-4-carboxylic acid amide

dimethyl sulfate

Downstream raw materials:

9-Methyl-8-methylthioxanthin

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