2-Methyl-6-(trideuteriomethyl)aniline

Base Information

Chemical Name:2-Methyl-6-(trideuteriomethyl)aniline
CAS No.:343272-28-6
Molecular Formula:C8H11N
Molecular Weight:124.198125334
Hs Code.:
European Community (EC) Number:693-953-2
DSSTox Substance ID:DTXSID10575895
Wikidata:Q82465338

Synonyms:343272-28-6;2-methyl-6-(trideuteriomethyl)aniline;DTXSID10575895;2-Methyl-6-(~2~H_3_)methylaniline;2,6-Dimethylaniline (2-methyl-d3), 99 atom % D, 95% (CP)

Suppliers and Price of 2-Methyl-6-(trideuteriomethyl)aniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
2,6-DIMETHYLANILINE(2-METHYL-D3) 95.00%
5MG
$ 499.26

Total 1 raw suppliers

Chemical Property of 2-Methyl-6-(trideuteriomethyl)aniline

Chemical Property:

PSA：26.02000
Density:1.01 g/mL at 25 °C
LogP:2.46680
XLogP3:1.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:124.107979593
Heavy Atom Count:9
Complexity:80.6

Purity/Quality:

95% by CP; 99% atom D ^*data from raw suppliers

2,6-DIMETHYLANILINE(2-METHYL-D3) 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C(=CC=C1)C)N
Isomeric SMILES:[2H]C([2H])([2H])C1=C(C(=CC=C1)C)N

Technology Process of 2-Methyl-6-(trideuteriomethyl)aniline

There total 1 articles about 2-Methyl-6-(trideuteriomethyl)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 4389-45-1
3-methylantranilic acid

: 343272-28-6
2-methyl-6-trideuteromethylaniline

Guidance literature:: With aluminium trichloride; lithium aluminium deuteride; In diethyl ether;
DOI:10.1016/S0040-4039(00)95920-3

Reference yield:

: 343272-28-6
2-methyl-6-trideuteromethylaniline

: C₉H₆⁽²⁾H₃NO

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) HNO₂, 2.) CuBr

2: 1.) Mg

3: 87 percent / SOCl₂

4: 1.) NH₂OH

5: methyl acetate / -43 °C / Irradiation; investigation of intramolecular insertion process; competition experiments; isotopeffect at various temperatures determined by NMR; ΔE_A

With thionyl chloride; hydroxylamine; cis-nitrous acid; magnesium; copper(I) bromide; In acetic acid methyl ester;
DOI:10.1016/S0040-4039(00)95920-3