Pentacyclo[11.4.4.34,10.07,23.015,19]tetracosa-2,4,6,8,10(22),11,13,15,17(1),18,20,23-dodecaene

Base Information

• Chemical Name: Pentacyclo[11.4.4.34,10.07,23.015,19]tetracosa-2,4,6,8,10(22),11,13,15,17(1),18,20,23-dodecaene
• CAS No.: 59456-90-5
• Molecular Weight: 304.38
• Mol file: 59456-90-5.mol

Synonyms:[2.2](2,6)(2,7)Naphthalenophane-1,11-diene;Pentacyclo[11.4.4.34,10.07,23.015,19]tetracosa-2,4,6,8,10(22),11,13,15,17(1),18,20,23-dodecaene

Chemical Property of Pentacyclo[11.4.4.34,10.07,23.015,19]tetracosa-2,4,6,8,10(22),11,13,15,17(1),18,20,23-dodecaene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Pentacyclo[11.4.4.34,10.07,23.015,19]tetracosa-2,4,6,8,10(22),11,13,15,17(1),18,20,23-dodecaene

There total 4 articles about Pentacyclo[11.4.4.34,10.07,23.015,19]tetracosa-2,4,6,8,10(22),11,13,15,17(1),18,20,23-dodecaene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C26H24O2S2 (69813-01-0) → <2.2>(2.6)Naphthalinophan-1.11-dien (59456-90-5)

Guidance literature:

at 500 ℃;

DOI:10.1016/0040-4020(78)89048-6

Reference yield:

C24H20S2 (59456-87-0) → <2.2>(2.6)Naphthalinophan-1.11-dien (59456-90-5)

Guidance literature:

Multi-step reaction with 3 steps

1: (i) nBuLi, (ii) /BRN= 969135/

2: NaIO₄

3: 500 °C

With sodium periodate;

DOI:10.1016/0040-4020(78)89048-6

Reference yield:

C26H24S2 (69812-99-3) → <2.2>(2.6)Naphthalinophan-1.11-dien (59456-90-5)

Guidance literature:

Multi-step reaction with 2 steps

1: NaIO₄

2: 500 °C

With sodium periodate;

DOI:10.1016/0040-4020(78)89048-6

upstream raw materials:

C₂₆H₂₄O₂S₂

C₂₄H₂₀S₂

C₂₆H₂₄S₂

Downstream raw materials:

<2.2> (2,6)naphthalenophane (achiral)