3-ethylbicyclo[3.2.0]hept-3-en-6-one

Base Information

Chemical Name:3-ethylbicyclo[3.2.0]hept-3-en-6-one
CAS No.:1235479-59-0
Molecular Formula:C₉H₁₂O
Molecular Weight:136.194
Hs Code.:
Mol file:1235479-59-0.mol

Synonyms:3-ethylbicyclo[3.2.0]hept-3-en-6-one

Suppliers and Price of 3-ethylbicyclo[3.2.0]hept-3-en-6-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Chemenu
3-ethylbicyclo[3.2.0]hept-3-en-6-one 95%+
1000g
$ 4000.00

Total 34 raw suppliers

Chemical Property of 3-ethylbicyclo[3.2.0]hept-3-en-6-one

Chemical Property:

Boiling Point:212.5±9.0 °C(Predicted)
PSA：17.07000
Density:1.043±0.06 g/cm3(Predicted)
LogP:1.93170

Purity/Quality:

99%, ^*data from raw suppliers

3-ethylbicyclo[3.2.0]hept-3-en-6-one 95%+ ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-ethylbicyclo[3.2.0]hept-3-en-6-one

There total 5 articles about 3-ethylbicyclo[3.2.0]hept-3-en-6-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1138245-49-4
4-Ethyl-3-hydroxyhept-6-enoic acid

: 1235479-59-0,1235479-61-4
3-ethylbicyclo[3.2.0]hept-3-ene-6-one

Guidance literature:: With potassium acetate; acetic anhydride; In acetic anhydride; at 20 ℃; for 10.1667h; Reflux;

Reference yield:

: 3249-68-1
ethyl butyroyl acetate

: 1235479-59-0,1235479-61-4
3-ethylbicyclo[3.2.0]hept-3-ene-6-one

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / tetrahydrofuran / 0.17 h / Cooling with ice

1.2: Cooling with ice

1.3: 5 h / 20 °C / Cooling with ice

2.1: sodium tetrahydroborate / ethanol / 2 h / Cooling with ice

2.2: 0.5 h

3.1: potassium hydroxide / methanol / 20 °C

3.3: Cooling with ice

4.1: acetic anhydride; potassium acetate / acetic anhydride / 10.17 h / 20 °C / Reflux

With sodium tetrahydroborate; potassium acetate; acetic anhydride; sodium hydride; potassium hydroxide; In tetrahydrofuran; methanol; ethanol; acetic anhydride;

Reference yield:

: 1138245-48-3
Ethyl 4-ethyl-3-hydroxyhept-6-enoate

: 1235479-59-0,1235479-61-4
3-ethylbicyclo[3.2.0]hept-3-ene-6-one

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hydroxide / methanol / 20 °C

1.3: Cooling with ice

2.1: acetic anhydride; potassium acetate / acetic anhydride / 10.17 h / 20 °C / Reflux

With potassium acetate; acetic anhydride; potassium hydroxide; In methanol; acetic anhydride;