FUMARIC-2,3-13C2 ACID

Base Information

• Chemical Name: FUMARIC-2,3-13C2 ACID
• CAS No.: 769108-94-3
• Molecular Formula: C₄H₄O₄
• Molecular Weight: 118.051
• Mol file: 769108-94-3.mol

Synonyms:FUMARIC-2,3-13C2 ACID;Fumaric acid-2,3-13C2

Chemical Property of FUMARIC-2,3-13C2 ACID

Chemical Property:

• Melting Point: 299-300 °C (subl.)(lit.)

Purity/Quality:

FUMARIC ACID-2,3-13C2 95.00% ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi
• Statements: 36
• Safety Statements: 26

MSDS Files:

Useful:

Technology Process of FUMARIC-2,3-13C2 ACID

There total 2 articles about FUMARIC-2,3-13C2 ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

di-tert-butyl fumarate → fumaric acid (769108-94-3)

Guidance literature:

With hydrogenchloride; In water; at 110 ℃; for 2h;

Reference yield:

[2,3-13C2]acetylenedicarboxylic acid (101391-58-6) → <2,3-(13)C2>succinic acid (61128-08-3) + <2,3-(13)C2>fumaric acid (769108-94-3)

Guidance literature:

With chromium (II); In water; Yield given. Yields of byproduct given. Title compound not separated from byproducts;

DOI:10.1002/hlca.19890720418

upstream raw materials:

[2,3-¹³C₂]acetylenedicarboxylic acid

Refernces

• 1、 Sandmeier,Tamm. "Studies on the biosynthesis of spirostaphylotrichin A". . p. 774 - 783. Retrieved 2007/10/02.