(14β)-12β-Acetyloxy-3β,14-dihydroxy-11α-[(1-oxo-3-phenyl-2-propenyl)oxy]pregnan-20-one

Base Information

• Chemical Name: (14β)-12β-Acetyloxy-3β,14-dihydroxy-11α-[(1-oxo-3-phenyl-2-propenyl)oxy]pregnan-20-one
• CAS No.: 55529-71-0
• Molecular Formula: C₃₂H₄₂O₇
• Molecular Weight: 538.681
• Mol file: 55529-71-0.mol

Synonyms:(14β)-12β-Acetyloxy-3β,14-dihydroxy-11α-[(1-oxo-3-phenyl-2-propenyl)oxy]pregnan-20-one

Chemical Property of (14β)-12β-Acetyloxy-3β,14-dihydroxy-11α-[(1-oxo-3-phenyl-2-propenyl)oxy]pregnan-20-one

Chemical Property:

• PSA: 110.13000
• LogP: 4.48680

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (14β)-12β-Acetyloxy-3β,14-dihydroxy-11α-[(1-oxo-3-phenyl-2-propenyl)oxy]pregnan-20-one

There total 3 articles about (14β)-12β-Acetyloxy-3β,14-dihydroxy-11α-[(1-oxo-3-phenyl-2-propenyl)oxy]pregnan-20-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Condurangoglycoside A0 (75316-69-7) → D-symarose (13089-76-4) + O-(6-deoxy-3-O-methyl-β-D-allopyranosyl)-(1→4)-O-D-oleandropyranose (19939-78-7) + condurangogenin A (55529-71-0) + neocondurangotriose

Guidance literature:

With oxonium; Further byproducts given;

DOI:10.1248/cpb.28.1954

Reference yield:

→ (E)-3-Phenyl-acrylic acid (8R,10S,11S,13S,14S)-12-acetoxy-17-acetyl-3,14-dihydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-11-yl ester (55529-71-0)

Guidance literature:

C39H54O10 II (Monosid A') (/BRN= 279749/, /BRN= 279750/), methanol. HCl, CHCl3;

DOI:10.1016/S0040-4020(01)98649-1

Reference yield:

→ (E)-3-Phenyl-acrylic acid (8R,10S,11S,13S,14S)-12-acetoxy-17-acetyl-3,14-dihydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-11-yl ester (55529-71-0)

Guidance literature:

'Kondurangogenin' (Verb. unbest. Kost., aus Kondurangorinde isoliert), n/10 H2SO4, Methanol (m. Cyclohexan ueberschichtet), Δ, Hydrolyse (neben anderen Verb., isoliert durch Saeulen- u. Schichtchromatogr.) (S. 1788, 1789, 1790, 1791);

DOI:10.1016/S0040-4020(01)98649-1

upstream raw materials:

Condurangoglycoside A₀

Downstream raw materials:

condurangogenin C

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