3-Fluoro-3-Methylazetidine hydrochloride

Base Information

• Chemical Name: 3-Fluoro-3-Methylazetidine hydrochloride
• CAS No.: 1427379-42-7
• Molecular Formula: C4H9ClFN
• Molecular Weight: 125.574
• Hs Code.: 2933998090
• Mol file: 1427379-42-7.mol

Synonyms:3-Fluoro-3-Methylazetidine hydrochloride;3-Fluoro-3-methylazetidine HCl

Chemical Property of 3-Fluoro-3-Methylazetidine hydrochloride

Chemical Property:

• PSA: 12.03000
• LogP: 1.44860
• Storage Temp.: Keep in dark place,Inert atmosphere,Store in freezer, under -20°C

Purity/Quality:

97% ^*data from raw suppliers

3-fluoro-3-methylazetidinehydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-Fluoro-3-Methylazetidine hydrochloride

There total 1 articles about 3-Fluoro-3-Methylazetidine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-benzyl-3-fluoro-3-methylazetidine (910795-88-9) → 3-fluoro-3-methylazetidine hydrochloride (1427379-42-7)

Guidance literature:

With hydrogenchloride; 10 wt% Pd(OH)2 on carbon; hydrogen; In 1,4-dioxane; ethanol; at 20 ℃; for 36h; under 1520.1 Torr;

Reference yield: 99.0%

3-fluoro-3-methylazetidine hydrochloride (1427379-42-7) + 2-(bromomethyl)-6-fluoro-benzonitrile → 2-fluoro-6-((3-fluoro-3-methylazetidin-1-yl)methyl)benzonitrile

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 12h;

Reference yield: 82.0%

3-fluoro-3-methylazetidine hydrochloride (1427379-42-7) + [2-bromo-7-{[(4-chlorophenyl)methyl]carbamoyl}-6-oxopyrido[2,3-b]pyrazin-5(6H)-yl]acetic acid → 2-bromo-N-[(4-chlorophenyl)methyl]-5-[2-(3-fluoro-3-methylazetidin-1-yl)-2-oxoethyl]-6-oxo-5,6-dihydropyrido[2,3-b]pyrazine-7-carboxamide

Guidance literature:

With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In N,N-dimethyl-formamide; for 1h; Cooling with ice;

upstream raw materials:

1-benzyl-3-fluoro-3-methylazetidine

Downstream raw materials:

C₂₄H₂₃ClFN₅O₄

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