4-((4-fluorotetrahydro-2H-pyran-4-yl)methoxy)-3-nitrobenzenesulfonamide

Base Information

Chemical Name:4-((4-fluorotetrahydro-2H-pyran-4-yl)methoxy)-3-nitrobenzenesulfonamide
CAS No.:1228838-56-9
Molecular Formula:C₁₂H₁₅FN₂O₆S
Molecular Weight:334.325
Hs Code.:
Mol file:1228838-56-9.mol

Synonyms:4-((4-fluorotetrahydro-2H-pyran-4-yl)methoxy)-3-nitrobenzenesulfonamide

Suppliers and Price of 4-((4-fluorotetrahydro-2H-pyran-4-yl)methoxy)-3-nitrobenzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-((4-fluorotetrahydro-2H-pyran-4-yl)methoxy)-3-nitrobenzenesulfonamide

Chemical Property:

Purity/Quality:

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Technology Process of 4-((4-fluorotetrahydro-2H-pyran-4-yl)methoxy)-3-nitrobenzenesulfonamide

There total 5 articles about 4-((4-fluorotetrahydro-2H-pyran-4-yl)methoxy)-3-nitrobenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 406233-31-6
4-fluoro-3-nitrobenzenesulfonamide

: 883442-46-4
(4-fluorotetrahydro-2H-pyran-4-yl) methanol

: 1228838-56-9
4-((4-fluorotetrahydro-2H-pyran-4-yl)methoxy)-3-nitrobenzenesulfonamide

Guidance literature:: With sodium hydride; In tetrahydrofuran; mineral oil;

Reference yield:

: 29943-42-8,143562-54-3
Tetrahydro-4H-pyran-4-one

: 1228838-56-9
4-((4-fluorotetrahydro-2H-pyran-4-yl)methoxy)-3-nitrobenzenesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: tert-butyl alcohol / 0.17 h

1.2: 16.66 h / 20 °C

2.1: pyridine hydrogenfluoride / dichloromethane / 4.5 h / 0 - 20 °C

3.1: water; sodium tetrahydroborate / isopropyl alcohol / 3 h / 0 - 20 °C

4.1: sodium hydride / tetrahydrofuran; mineral oil

With sodium tetrahydroborate; water; sodium hydride; pyridine hydrogenfluoride; In tetrahydrofuran; dichloromethane; isopropyl alcohol; mineral oil; tert-butyl alcohol;

Reference yield:

: 883442-47-5
1,6-dioxaspiro[2.5]octane-2-carbonitrile

: 1228838-56-9
4-((4-fluorotetrahydro-2H-pyran-4-yl)methoxy)-3-nitrobenzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine hydrogenfluoride / dichloromethane / 4.5 h / 0 - 20 °C

2: water; sodium tetrahydroborate / isopropyl alcohol / 3 h / 0 - 20 °C

3: sodium hydride / tetrahydrofuran; mineral oil

With sodium tetrahydroborate; water; sodium hydride; pyridine hydrogenfluoride; In tetrahydrofuran; dichloromethane; isopropyl alcohol; mineral oil;