3-(BOC-AMINO)-3-METHYLAZETIDINE

Base Information

• Chemical Name: 3-(BOC-AMINO)-3-METHYLAZETIDINE
• CAS No.: 1018443-01-0
• Molecular Formula: C9H18N2O2
• Molecular Weight: 186.254
• Hs Code.: 2933990090
• Mol file: 1018443-01-0.mol

Synonyms:3-(BOC-AMINO)-3-METHYLAZETIDINE;3-(Boc-aMino)-3-Methylaze...;tert-Butyl (3-methylazetidin-3-yl)carbamate;(3-Methyl-azetidin-3-yl)-carbamic acid tert-butyl ester

Chemical Property of 3-(BOC-AMINO)-3-METHYLAZETIDINE

Chemical Property:

• Boiling Point: 270.6±29.0 °C(Predicted)
• PKA: 10.26±0.20(Predicted)
• PSA: 53.85000
• Density: 1.04±0.1 g/cm3(Predicted)
• LogP: 1.40620
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

(3-Methyl-azetidin-3-yl)-carbamicacidtert-butylester 96% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-(BOC-AMINO)-3-METHYLAZETIDINE

There total 1 articles about 3-(BOC-AMINO)-3-METHYLAZETIDINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

(1-benzhydryl-3-methyl-azetidin-3-yl)-carbamic acid tert-butyl ester (920320-54-3) → tert-butyl N-(3-methylazetidin-3-yl)carbamate (1018443-01-0)

Guidance literature:

With hydrogen; palladium hydroxide on carbon; In ethanol; ethyl acetate; at 60 ℃; under 2585.81 Torr;

Reference yield: 53.0%

tert-butyl N-(3-methylazetidin-3-yl)carbamate (1018443-01-0) + benzyl chloroformate (501-53-1,94274-21-2) → benzyl 3-((tert-butoxy-carbonyl)amino)-3-methylazetidin-1-carboxylate

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 20 ℃; for 3h;

upstream raw materials:

(1-benzhydryl-3-methyl-azetidin-3-yl)-carbamic acid tert-butyl ester

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