2-Methyl-4-[(4-methylphenyl)hydrazinylidene]cyclohexa-2,5-dien-1-one

Base Information

Chemical Name:2-Methyl-4-[(4-methylphenyl)hydrazinylidene]cyclohexa-2,5-dien-1-one
CAS No.:21462-92-0
Molecular Formula:C14H14N2O
Molecular Weight:226.278
Hs Code.:2927000090
NSC Number:83597
DSSTox Substance ID:DTXSID60418283
Nikkaji Number:J2.070.020C
Mol file:21462-92-0.mol

Synonyms:21462-92-0;2-methyl-4-[(4-methylphenyl)hydrazinylidene]cyclohexa-2,5-dien-1-one;NSC83597;DTXSID60418283;NSC-83597;2-methyl-4-[(4-methylphenyl)diazenyl]phenol

Suppliers and Price of 2-Methyl-4-[(4-methylphenyl)hydrazinylidene]cyclohexa-2,5-dien-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 2-Methyl-4-[(4-methylphenyl)hydrazinylidene]cyclohexa-2,5-dien-1-one

Chemical Property:

Vapor Pressure:3.7E-05mmHg at 25°C
Boiling Point:353°Cat760mmHg
Flash Point:167.3°C
PSA：41.46000
Density:1.09g/cm³
LogP:2.92110
XLogP3:3.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:226.110613074
Heavy Atom Count:17
Complexity:259

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)N=NC2=CC(=C(C=C2)O)C

Technology Process of 2-Methyl-4-[(4-methylphenyl)hydrazinylidene]cyclohexa-2,5-dien-1-one

There total 6 articles about 2-Methyl-4-[(4-methylphenyl)hydrazinylidene]cyclohexa-2,5-dien-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 106-49-0,12221-03-3
p-toluidine

: 95-48-7,77504-84-8
ortho-cresol

: 21462-92-0
2-Methyl-4-p-tolylazo-phenol

Guidance literature:: p-toluidine; With hydrogenchloride; sodium nitrite; In water; at 0 - 5 ℃;

ortho-cresol; With sodium hydroxide; In water; at 0 - 5 ℃; pH=8 - 8.5;
DOI:10.1080/15421406.2010.504632

Reference yield:

: benzoic acid-[(3-methyl-4-oxo-cyclohexa-2,5-dienylidene)-p-tolyl-hydrazide]

: 21462-92-0
2-Methyl-4-p-tolylazo-phenol

Guidance literature:: With sulfuric acid;

Reference yield:

: 553-97-9
2-Methyl-1,4-benzoquinone

: 21462-92-0
2-Methyl-4-p-tolylazo-phenol

Guidance literature:: Multi-step reaction with 2 steps

1: diluted alcohol

2: concentrated sulfuric acid

With ethanol; sulfuric acid;