10,11-DIHYDRO-DIBENZO[B,F][1,4]OXAZEPINE

Base Information

Chemical Name:10,11-DIHYDRO-DIBENZO[B,F][1,4]OXAZEPINE
CAS No.:2244-60-2
Molecular Formula:C13H11NO
Molecular Weight:197.236
Hs Code.:2934999090
Mol file:2244-60-2.mol

Synonyms:10,11-DIHYDRO-DIBENZO[B,F][1,4]OXAZEPINE

Suppliers and Price of 10,11-DIHYDRO-DIBENZO[B,F][1,4]OXAZEPINE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
10,11-Dihydrodibenzo[B,F][1,4]oxazepine
50mg
$ 110.00

Matrix Scientific
10,11-Dihydro-dibenzo[b,f][1,4]oxazepine
1g
$ 378.00

Crysdot
10,11-Dihydrodibenzo[b,f][1,4]oxazepine 95+%
1g
$ 370.00

American Custom Chemicals Corporation
10,11-DIHYDRO-DIBENZO[B,F][1,4]OXAZEPINE 95.00%
500MG
$ 768.08

Alichem
10,11-Dihydrodibenzo[b,f][1,4]oxazepine
1g
$ 378.00

Alichem
10,11-Dihydrodibenzo[b,f][1,4]oxazepine
250mg
$ 161.57

Alichem
10,11-Dihydrodibenzo[b,f][1,4]oxazepine
5g
$ 1389.15

AK Scientific
10,11-Dihydro-dibenzo[b,f][1,4]oxazepine
1g
$ 560.00

Total 10 raw suppliers

Chemical Property of 10,11-DIHYDRO-DIBENZO[B,F][1,4]OXAZEPINE

Chemical Property:

PSA：21.26000
LogP:3.54240

Purity/Quality:

98%min ^*data from raw suppliers

10,11-Dihydrodibenzo[B,F][1,4]oxazepine ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:Xi

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 10,11-DIHYDRO-DIBENZO[B,F][1,4]OXAZEPINE

There total 6 articles about 10,11-DIHYDRO-DIBENZO[B,F][1,4]OXAZEPINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 3158-85-8
10H-dibenzo[b,f][1,4]oxazepin-11-one

: 2244-60-2
10,11-dihydrodibenz[b,f][1,4]oxazepine

Guidance literature:: With dimethylsulfide borane complex; In tetrahydrofuran; for 3h; Reflux;

Reference yield:

: 2244-59-9
8-chloro-10,11-dihydrodibenz[b,f][1,4]oxazepine

: 2244-60-2
10,11-dihydrodibenz[b,f][1,4]oxazepine

Guidance literature:: With sodium hydroxide; hydrogen; palladium; In ethanol; chloroform;

Reference yield:

: 666818-15-1
2-fluoro-N-(2-hydroxyphenyl)-benzamide

: 2244-60-2
10,11-dihydrodibenz[b,f][1,4]oxazepine

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / N,N-dimethyl-formamide / 5 h / 120 °C

2: lithium aluminium tetrahydride / tetrahydrofuran / 70 °C

With lithium aluminium tetrahydride; sodium hydroxide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1039/c5ob00439j