2-(4-broMophenyl)-5,8-dioxaspiro[3.4]octane-2-carbonitrile

Base Information

• Chemical Name: 2-(4-broMophenyl)-5,8-dioxaspiro[3.4]octane-2-carbonitrile
• CAS No.: 1227958-64-6
• Molecular Formula: C13H12BrNO2
• Molecular Weight: 294.148
• Mol file: 1227958-64-6.mol

Synonyms:2-(4-broMophenyl)-5,8-dioxaspiro[3.4]octane-2-carbonitrile

Chemical Property of 2-(4-broMophenyl)-5,8-dioxaspiro[3.4]octane-2-carbonitrile

Chemical Property:

• PSA: 42.25000
• LogP: 2.74738

Purity/Quality:

2-(4-Bromophenyl)-5,8-dioxaspiro-[3.4]octane-2-carbonitrile 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-(4-broMophenyl)-5,8-dioxaspiro[3.4]octane-2-carbonitrile

There total 1 articles about 2-(4-broMophenyl)-5,8-dioxaspiro[3.4]octane-2-carbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,2-bis(bromomethyl)-1,3-dioxolane (20599-01-3) + 4-Bromophenylacetonitrile (16532-79-9) → 2-(4-bromophenyl)-5,8-dioxaspiro[3.4]octane-2-carbonitrile (1227958-64-6)

Guidance literature:

4-Bromophenylacetonitrile; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 ℃;

2,2-bis(bromomethyl)-1,3-dioxolane; In N,N-dimethyl-formamide; mineral oil; at 0 - 60 ℃; for 16.33h;

With methanol; In N,N-dimethyl-formamide; mineral oil; at 0 ℃;

Reference yield:

2-(4-bromophenyl)-5,8-dioxaspiro[3.4]octane-2-carbonitrile (1227958-64-6) → 2-(4-bromophenyl)-5,8-dioxaspiro[3.4]octane-2-carboxylic acid amide (1245770-20-0)

Guidance literature:

With ammonium hydroxide; dihydrogen peroxide; In methanol; water; at 20 ℃; for 16h;

upstream raw materials:

2,2-bis(bromomethyl)-1,3-dioxolane

4-Bromophenylacetonitrile

Downstream raw materials:

2-(4-bromophenyl)-5,8-dioxaspiro[3.4]octane-2-carboxylic acid amide

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