2,5-Difluoro-4-iodoaniline

Base Information

• Chemical Name: 2,5-Difluoro-4-iodoaniline
• CAS No.: 155906-13-1
• Molecular Formula: C6H4F2IN
• Molecular Weight: 255.006
• Hs Code.: 2921420090
• Mol file: 155906-13-1.mol

Synonyms:2,5-Difluoro-4-iodoaniline

Chemical Property of 2,5-Difluoro-4-iodoaniline

Chemical Property:

• PSA: 26.02000
• LogP: 2.73280
• Storage Temp.: 2-8°C(protect from light)

Purity/Quality:

97% ^*data from raw suppliers

2,5-Difluoro-4-iodoaniline 96% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,5-Difluoro-4-iodoaniline

There total 2 articles about 2,5-Difluoro-4-iodoaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

2,5-difluoroaniline (367-30-6) → 2,5-difluoro-4-iodophenylamine (155906-13-1)

Guidance literature:

With iodine; sodium hydrogencarbonate; In water; at 20 ℃; for 2h;

DOI:10.1016/j.jfluchem.2016.06.010

Reference yield: 71.0%

4-bromo-2,5-difluoroaniline (112279-60-4) → 2,5-difluoro-4-iodophenylamine (155906-13-1)

Guidance literature:

With copper(l) iodide; N,N-dimethylethylenediamine; sodium iodide; In 1,4-dioxane; at 140 ℃; for 3h; Inert atmosphere;

DOI:10.1021/jm301549a

Reference yield: 98.0%

bis(trichloromethyl) carbonate (32315-10-9) + 2,5-difluoro-4-iodophenylamine (155906-13-1) → 2,5-difluoro-4-iodophenylisocyanate

Guidance literature:

With triethylamine; In benzene; for 4h; Reflux;

DOI:10.1016/j.tet.2018.02.062

upstream raw materials:

2,5-difluoroaniline

4-bromo-2,5-difluoroaniline

Downstream raw materials:

4-[5-(((p-chlorobenzoyl)oxy)methyl)-4-(benzyloxy)-2,5-dihydro-β-L-furan-2-yl]-2,5-difluoroaniline

2,5-difluoro-4-(β-D-glycero-pentofuran-3-ulos-1-yl)aniline

N-(2,5-difluoro-4-iodophenyl)methanesulfonamide

8-(3-phenyl[1,2,4]oxadiazol-5-yl)-1-oxa-2,8-diazaspiro[4.5]-dec-2-ene-3-carboxylic acid (2,5-difluoro-4-methylsulfanylphenyl)amide

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