3,4-Didehydro-1,2,7',8',11',12'-hexahydro-1-methoxy-ψ,ψ-carotene

Base Information

Chemical Name:3,4-Didehydro-1,2,7',8',11',12'-hexahydro-1-methoxy-ψ,ψ-carotene
CAS No.:22076-59-1
Molecular Formula:C41H62O
Molecular Weight:570.93038
Hs Code.:
Mol file:22076-59-1.mol

Synonyms:11',12'-Dihydrospheroidene;3,4-Didehydro-1,2,7',8',11',12'-hexahydro-1-methoxy-ψ,ψ-carotene

Suppliers and Price of 3,4-Didehydro-1,2,7',8',11',12'-hexahydro-1-methoxy-ψ,ψ-carotene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 3,4-Didehydro-1,2,7',8',11',12'-hexahydro-1-methoxy-ψ,ψ-carotene

Chemical Property:

PSA：9.23000
LogP:13.01090

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3,4-Didehydro-1,2,7',8',11',12'-hexahydro-1-methoxy-ψ,ψ-carotene

There total 18 articles about 3,4-Didehydro-1,2,7',8',11',12'-hexahydro-1-methoxy-ψ,ψ-carotene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 52062-29-0
1-methoxy-1,2,7',8',11',12'-hexahydro-ψ,ψ-caroten-4-one

: 22076-59-1
11',12'-dihydrospheroidene

Guidance literature:: Multi-step reaction with 2 steps

1: KBH₄ / ethanol

2: aq. HCl, CHCl₃ / 0.03 h

With hydrogenchloride; potassium borohydride; chloroform; In ethanol;

Reference yield:

: 52062-38-1
1-methoxy-1,2,7',8',11',12'-hexahydro-ψ,ψ-caroten-4-ol

: 22076-59-1
11',12'-dihydrospheroidene

Guidance literature:: With hydrogenchloride; chloroform; for 0.0333333h;

Reference yield:

: 1117-52-8
6,10,14-trimethyl-5,9,13-pentadecatriene-2-on

: 22076-59-1
11',12'-dihydrospheroidene

Guidance literature:: Multi-step reaction with 7 steps

1: 1) BuLi / 1) THF, -30 to 0 deg C, 10 min, 2) THF, r.t., 30 min

2: 1) Dibal, 2) H₂O, silica gel / 1) petroleum ether, -78 to 0 deg C, 30 min, 2) 0 deg C, 1 h

3: 1) BuLi / 1) THF, 0 deg C, 15 min, 2) THF, r.t., 10 min

4: 1) Dibal, 2) H₂O, silica gel / 1) petroleum ether, -78 to 0 deg C, 30 min, 2) 0 deg C, 1 h

5: 1) BuLi / 1) THF, 0 deg C, 15 min, 2) THF, r.t., 10 min

6: 1) Dibal, 2) H₂O, silica gel / 1) petroleum ether, -78 to 0 deg C, 30 min, 2) 0 deg C, 1 h

7: 1) BuLi / 1) THF, -30 deg C to r.t., 2) THF, r.t., 1.5 h

With n-butyllithium; water; silica gel; diisobutylaluminium hydride;