beta-L-erythro-Hex-4-enopyranoside, methyl 6-amino-4,6-dideoxy- (9CI)

Base Information

Chemical Name:beta-L-erythro-Hex-4-enopyranoside, methyl 6-amino-4,6-dideoxy- (9CI)
CAS No.:651302-64-6
Molecular Formula:C7H13NO4
Molecular Weight:175.18242
Hs Code.:
Mol file:651302-64-6.mol

Synonyms:beta-L-erythro-Hex-4-enopyranoside, methyl 6-amino-4,6-dideoxy- (9CI)

Suppliers and Price of beta-L-erythro-Hex-4-enopyranoside, methyl 6-amino-4,6-dideoxy- (9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of beta-L-erythro-Hex-4-enopyranoside, methyl 6-amino-4,6-dideoxy- (9CI)

Chemical Property:

Purity/Quality:

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Technology Process of beta-L-erythro-Hex-4-enopyranoside, methyl 6-amino-4,6-dideoxy- (9CI)

There total 3 articles about beta-L-erythro-Hex-4-enopyranoside, methyl 6-amino-4,6-dideoxy- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 651302-27-1
methyl 2,3-di-O-benzoyl-4,6-dideoxy-6-amino-β-L-erythro-hex-4-enopyranoside

: 651302-64-6
methyl 4,6-dideoxy-6-amino-β-L-erythro-hex-4-enopyranoside

Guidance literature:: With potassium carbonate; In methanol; at 20 ℃; for 2.5h;
DOI:10.1081/CAR-120026469

Reference yield:

: 34234-44-1,53182-61-9,88037-32-5,101194-17-6,120104-44-1,120104-49-6
methyl 2,3,4-tri-O-benzoyl-α-D-mannopyranoside

: 651302-64-6
methyl 4,6-dideoxy-6-amino-β-L-erythro-hex-4-enopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 58 percent / silica gel; PCC / toluene / 36 h / Heating

2: 28 percent / ammonium acetate; NaBH₃CN; molecular sieves 3 Angstroem / methanol / 14.5 h / 20 °C

3: 48 percent / K₂CO₃ / methanol / 2.5 h / 20 °C

With ammonium acetate; 3 A molecular sieve; silica gel; sodium cyanoborohydride; potassium carbonate; pyridinium chlorochromate; In methanol; toluene;
DOI:10.1081/CAR-120026469

Reference yield:

: 553662-29-6
methyl 2,3-di-O-benzoyl-4-deoxy-6-aldehydo-β-L-erythro-hex-4-enopyranoside

: 651302-64-6
methyl 4,6-dideoxy-6-amino-β-L-erythro-hex-4-enopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 28 percent / ammonium acetate; NaBH₃CN; molecular sieves 3 Angstroem / methanol / 14.5 h / 20 °C

2: 48 percent / K₂CO₃ / methanol / 2.5 h / 20 °C

With ammonium acetate; 3 A molecular sieve; sodium cyanoborohydride; potassium carbonate; In methanol;
DOI:10.1081/CAR-120026469