6,7-dihydro-3-Methyl-5H-Pyrrolo[2,1-c]-1,2,4-triazole-7-carboxylic acid

Base Information

Chemical Name:6,7-dihydro-3-Methyl-5H-Pyrrolo[2,1-c]-1,2,4-triazole-7-carboxylic acid
CAS No.:1190392-04-1
Molecular Formula:C₇H₉N₃O₂
Molecular Weight:167.167
Hs Code.:
Mol file:1190392-04-1.mol

Synonyms:6,7-dihydro-3-Methyl-5H-Pyrrolo[2,1-c]-1,2,4-triazole-7-carboxylic acid;3-methyl-6,7-dihydro-5H-pyrrolo[2,1-c][1,2,4]triazole-7-carboxylic acid

Suppliers and Price of 6,7-dihydro-3-Methyl-5H-Pyrrolo[2,1-c]-1,2,4-triazole-7-carboxylic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Matrix Scientific
3-Methyl-6,7-dihydro-5H-pyrrolo-[2,1-c][1,2,4]triazole-7-carboxylic acid 95+%
1g
$ 3036.00

Crysdot
3-Methyl-6,7-dihydro-5H-pyrrolo-[2,1-c][1,2,4]triazole-7-carboxylicacid 95+%
1g
$ 1784.00

Total 5 raw suppliers

Chemical Property of 6,7-dihydro-3-Methyl-5H-Pyrrolo[2,1-c]-1,2,4-triazole-7-carboxylic acid

Chemical Property:

PSA：68.01000
LogP:0.15840

Purity/Quality:

97% ^*data from raw suppliers

3-Methyl-6,7-dihydro-5H-pyrrolo-[2,1-c][1,2,4]triazole-7-carboxylic acid 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 6,7-dihydro-3-Methyl-5H-Pyrrolo[2,1-c]-1,2,4-triazole-7-carboxylic acid

There total 3 articles about 6,7-dihydro-3-Methyl-5H-Pyrrolo[2,1-c]-1,2,4-triazole-7-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1190392-05-2
ethyl 3-methyl-6,7-dihydro-5H-pyrrolo[2,1-c][1,2,4]-triazole-7-carboxylate

: 1190392-04-1
3-methyl-6,7-dihydro-5H-pyrrolo[2,1-c][1,2,4]-triazole-7-carboxylic acid

Guidance literature:: ethyl 3-methyl-6,7-dihydro-5H-pyrrolo[2,1-c][1,2,4]-triazole-7-carboxylate; With water; lithium hydroxide; In tetrahydrofuran; methanol; at 60 ℃; for 16h;

With hydrogenchloride; In water; pH=~ 5;

Reference yield:

: 36821-26-8
2-oxopyrrolidine-3-carboxylic acid ethyl ester

: 1190392-04-1
3-methyl-6,7-dihydro-5H-pyrrolo[2,1-c][1,2,4]-triazole-7-carboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: trimethoxonium tetrafluoroborate / dichloromethane / 2 h / 20 °C

1.2: 3 h / 20 °C

1.3: 120 °C

2.1: water; lithium hydroxide / tetrahydrofuran; methanol / 16 h / 60 °C

2.2: pH ~ 5

With water; trimethoxonium tetrafluoroborate; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane;

Reference yield:

: ethyl 5-methoxy-3,4-dihydro-2H-pyrrole-4-carboxylate

: 1190392-04-1
3-methyl-6,7-dihydro-5H-pyrrolo[2,1-c][1,2,4]-triazole-7-carboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: dichloromethane / 3 h / 20 °C

2.1: water; lithium hydroxide / tetrahydrofuran; methanol / 16 h / 60 °C

2.2: pH 5

With water; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane;