CIS-(Z)-8-AMINO-CYCLOOCT-4-ENECARBOXYLIC ACID

Base Information

• Chemical Name: CIS-(Z)-8-AMINO-CYCLOOCT-4-ENECARBOXYLIC ACID
• CAS No.: 736127-53-0
• Molecular Formula: C₉H₁₅NO₂
• Molecular Weight: 169.224
• Mol file: 736127-53-0.mol

Synonyms:CIS-(Z)-8-AMINO-CYCLOOCT-4-ENECARBOXYLIC ACID

Chemical Property of CIS-(Z)-8-AMINO-CYCLOOCT-4-ENECARBOXYLIC ACID

Chemical Property:

• Vapor Pressure: 0.000107mmHg at 25°C
• Boiling Point: 313.6°C at 760 mmHg
• Flash Point: 143.4°C
• PSA: 63.32000
• Density: 1.091g/cm³
• LogP: 1.84500

Purity/Quality:

99% ^*data from raw suppliers

CIS-(Z)-8-AMINO-CYCLOOCT-4-ENECARBOXYLIC ACID 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of CIS-(Z)-8-AMINO-CYCLOOCT-4-ENECARBOXYLIC ACID

There total 6 articles about CIS-(Z)-8-AMINO-CYCLOOCT-4-ENECARBOXYLIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

(±)-(Z)-9-azabicyclo[6.2.0]dec-4-en-10-one → (1S,8R,4Z)-9-azabicyclo[6.2.0]dec-4-en-10-one + (Z)-(1R,8S)-8-Amino-cyclooct-4-enecarboxylic acid (807314-37-0,736127-53-0)

Guidance literature:

With lipase*from*Candida*ntarctica; In di-isopropyl ether; water; at 60 ℃; for 72h; Resolution of racemate; Enzymatic reaction;

DOI:10.1039/c4ob00266k

Reference yield: 47.0%

(±)-(Z)-9-azabicyclo[6.2.0]dec-4-en-10-one → (1S,8R,4Z)-9-azabicyclo[6.2.0]dec-4-en-10-one + (Z)-(1S,8R)-8-Amino-cyclooct-4-enecarboxylic acid (807314-37-0,736127-53-0) + (Z)-(1R,8S)-8-Amino-cyclooct-4-enecarboxylic acid (807314-37-0,736127-53-0)

Guidance literature:

With Candida antarctica lipase B on resin; In di-isopropyl ether; water; at 70 ℃; for 7h;

DOI:10.1016/j.tetasy.2004.05.029

Reference yield: 47.0%

(±)-(Z)-9-azabicyclo[6.2.0]dec-4-en-10-one → (1S,8R,4Z)-9-azabicyclo[6.2.0]dec-4-en-10-one + (Z)-(1S,8R)-8-Amino-cyclooct-4-enecarboxylic acid (807314-37-0,736127-53-0) + (Z)-(1R,8S)-8-Amino-cyclooct-4-enecarboxylic acid (807314-37-0,736127-53-0)

Guidance literature:

With Candida antarctica lipase B on resin; In di-isopropyl ether; water; at 70 ℃; for 7h;

DOI:10.1016/j.tetasy.2004.05.029

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