5-PyriMidinecarboxylic acid, 2-[4-(phenylMethyl)-1-piperazinyl]-, Methyl ester

Base Information

• Chemical Name: 5-PyriMidinecarboxylic acid, 2-[4-(phenylMethyl)-1-piperazinyl]-, Methyl ester
• CAS No.: 1133784-12-9
• Molecular Formula: C₁₇H₂₀N₄O₂
• Molecular Weight: 312.371
• Hs Code.: 2933990090
• Mol file: 1133784-12-9.mol

Synonyms:5-PyriMidinecarboxylic acid, 2-[4-(phenylMethyl)-1-piperazinyl]-, Methyl ester

Chemical Property of 5-PyriMidinecarboxylic acid, 2-[4-(phenylMethyl)-1-piperazinyl]-, Methyl ester

Chemical Property:

• PSA: 58.56000
• LogP: 1.58830

Purity/Quality:

Methyl2-(4-benzylpiperazin-1-yl)pyrimidine-5-carboxylate 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5-PyriMidinecarboxylic acid, 2-[4-(phenylMethyl)-1-piperazinyl]-, Methyl ester

There total 1 articles about 5-PyriMidinecarboxylic acid, 2-[4-(phenylMethyl)-1-piperazinyl]-, Methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-benzylpiperazine-1-carboximidamide (7773-69-5,105735-38-4) + sodium 2-(dimethoxymethyl)-3-methoxy-3-oxoprop-1-en-1-olate → Methyl 2-(4-benzylpiperazin-1-yl)pyrimidine-5-carboxylate (1133784-12-9)

Guidance literature:

In N,N-dimethyl-formamide; at 10 ℃;

Reference yield: 77.0%

Methyl 2-(4-benzylpiperazin-1-yl)pyrimidine-5-carboxylate (1133784-12-9) → Methyl 2-(piperazin-1-yl)pyrimidine-5-carboxylate (1057682-19-5)

Guidance literature:

With hydrogen; palladium 10% on activated carbon; In 1,4-dioxane; methanol; at 20 ℃; for 24h;

upstream raw materials:

4-benzylpiperazine-1-carboximidamide

Downstream raw materials:

Methyl 2-(piperazin-1-yl)pyrimidine-5-carboxylate

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