(Benzylideneamino)diphenylphosphine sulfide

Base Information

• Chemical Name: (Benzylideneamino)diphenylphosphine sulfide
• CAS No.: 58156-56-2
• Molecular Formula: C₁₉H₁₆NPS
• Molecular Weight: 321.383
• Mol file: 58156-56-2.mol

Synonyms:(Benzylideneamino)diphenylphosphine sulfide;Diphenyl(phenylmethyleneamino)phosphine sulfide;N-(Diphenylthiophophinyl)benzenemethaneimine

Chemical Property of (Benzylideneamino)diphenylphosphine sulfide

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (Benzylideneamino)diphenylphosphine sulfide

There total 2 articles about (Benzylideneamino)diphenylphosphine sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

(diethoxymethyl)benzene (774-48-1) + P,P-diphenylphosphinothioic amide (17366-80-2) → N-benzylidene-diphenylthiophosphinamide (58156-56-2)

Guidance literature:

at 120 - 160 ℃;

DOI:10.1002/hc.20412

Reference yield:

→ N-benzylidene-diphenylthiophosphinamide (58156-56-2)

Guidance literature:

Phosphoranyl-Methylazid 1, Thermolyse;

Reference yield: 98.0%

nitromethane (75-52-5) + N-benzylidene-diphenylthiophosphinamide (58156-56-2) → C20H19N2O2PS (1201630-07-0)

Guidance literature:

With N,N,N',N'-tetramethylguanidine; at 20 ℃; for 0.166667h; Neat (no solvent);

DOI:10.1016/j.tetasy.2009.08.025

upstream raw materials:

(diethoxymethyl)benzene

P,P-diphenylphosphinothioic amide

Downstream raw materials:

C₂₃H₂₂NOPS

C₂₃H₂₂NO₂PS

C₂₀H₁₉N₂O₂PS

(3R)-3-amino-3-phenylpropanenitrile