(E)-ethyl 3-(3-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)phenyl)acrylate

Base Information

Chemical Name:(E)-ethyl 3-(3-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)phenyl)acrylate
CAS No.:1377024-34-4
Molecular Formula:C17H23BO4
Molecular Weight:302.17312
Hs Code.:
Mol file:1377024-34-4.mol

Synonyms:(E)-ethyl 3-(3-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)phenyl)acrylate

Suppliers and Price of (E)-ethyl 3-(3-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)phenyl)acrylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 4 raw suppliers

Chemical Property of (E)-ethyl 3-(3-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)phenyl)acrylate

Chemical Property:

Boiling Point:421.9±28.0 °C(Predicted)
Density:1.06±0.1 g/cm3(Predicted)

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (E)-ethyl 3-(3-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)phenyl)acrylate

There total 6 articles about (E)-ethyl 3-(3-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)phenyl)acrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 480425-35-2
methyl 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzoate

: 867-13-0
diethoxyphosphoryl-acetic acid ethyl ester

: 1377024-34-4
ethyl (E)-3-[3-(4,4,5,5-tetramethyl-1,3-dioxaborolan-2-yl)phenyl]acrylate

Guidance literature:: methyl 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzoate; With {μ-ClIr(cyclooctene)2}2; H₂SiEt₂; In dichloromethane; at 20 ℃; for 8h; Inert atmosphere;

diethoxyphosphoryl-acetic acid ethyl ester; With potassium trimethylsilonate; In tetrahydrofuran; at 20 ℃; for 0.5h;
DOI:10.1021/acs.orglett.5b02901

Reference yield: 67.0%

: 76-09-5
2,3-dimethyl-2,3-butane diol

: C₂₅H₂₅BN₂O₇

: C₁₄H₁₆N₂O₅

: 1377024-34-4
C₁₇H₂₃BO₄

Guidance literature:: With potassium phosphate; In dichloromethane; water; at 20 ℃; for 18h;
DOI:10.1039/d0sc00230e

Reference yield:

: 867-13-0
diethoxyphosphoryl-acetic acid ethyl ester

: 380151-86-0
3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenylcarboxaldehyde

: 1377024-34-4
ethyl (E)-3-[3-(4,4,5,5-tetramethyl-1,3-dioxaborolan-2-yl)phenyl]acrylate

Guidance literature:: diethoxyphosphoryl-acetic acid ethyl ester; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 ℃; for 0.5h; Inert atmosphere;

3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenylcarboxaldehyde; In tetrahydrofuran; mineral oil; at 0 ℃; for 1h; Inert atmosphere;
DOI:10.1016/j.tet.2015.05.107