1,3-DibroMo-5-hexyl-4H-thieno[3,4-c]pyrrole-4,6(5H)-dione

Base Information

Chemical Name:1,3-DibroMo-5-hexyl-4H-thieno[3,4-c]pyrrole-4,6(5H)-dione
CAS No.:566939-56-8
Molecular Formula:C12H13Br2NO2S
Molecular Weight:395.11012
Hs Code.:2934999090
Mol file:566939-56-8.mol

Synonyms:1,3-DibroMo-5-hexyl-4H-thieno[3,4-c]pyrrole-4,6(5H)-dione

Suppliers and Price of 1,3-DibroMo-5-hexyl-4H-thieno[3,4-c]pyrrole-4,6(5H)-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
1,3-DIBROMO-5-HEXYL-4H-THIENO[3,4-C]PYRROLE-4,6(5H)-DIONE 95.00%
5MG
$ 505.45

Alichem
1,3-Dibromo-5-hexyl-4H-thieno[3,4-c]pyrrole-4,6(5H)-dione
1g
$ 783.36

Total 14 raw suppliers

Chemical Property of 1,3-DibroMo-5-hexyl-4H-thieno[3,4-c]pyrrole-4,6(5H)-dione

Chemical Property:

PSA：65.62000
LogP:4.38730
Storage Temp.:2-8°C

Purity/Quality:

98% ^*data from raw suppliers

1,3-DIBROMO-5-HEXYL-4H-THIENO[3,4-C]PYRROLE-4,6(5H)-DIONE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1,3-DibroMo-5-hexyl-4H-thieno[3,4-c]pyrrole-4,6(5H)-dione

There total 8 articles about 1,3-DibroMo-5-hexyl-4H-thieno[3,4-c]pyrrole-4,6(5H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.23%

: 6007-85-8
1H,3H-thieno[3,4-c]furan-1,3-dione

: 111-26-2
hexan-1-amine

: 566939-56-8
1,3-dibromo-5-(n-hexyl)-4H-thieno[3,4-c]pyrrole-4,6(5H)-dione

Guidance literature:: 1H,3H-thieno[3,4-c]furan-1,3-dione; hexan-1-amine; In toluene; at 120 ℃; for 24h; Inert atmosphere;

With pyridine; sulfurous dibromide; In toluene; at 0 - 120 ℃; for 29h; Inert atmosphere;

Reference yield: 90.0%

: 566939-54-6
5-hexyl-4H-thieno[3,4-c]pyrrole-4,6(5H)-dione

: 566939-56-8
1,3-dibromo-5-(n-hexyl)-4H-thieno[3,4-c]pyrrole-4,6(5H)-dione

Guidance literature:: With N-Bromosuccinimide; sulfuric acid; trifluoroacetic acid; at 20 ℃; for 12h;
DOI:10.1021/acs.inorgchem.0c02468

Reference yield: 82.0%

: 111-26-2
hexan-1-amine

: 1015423-45-6
2,5-dibromothiophene-3,4-dicarboxylic acid anhydryde

: 566939-56-8
1,3-dibromo-5-(n-hexyl)-4H-thieno[3,4-c]pyrrole-4,6(5H)-dione

Guidance literature:: hexan-1-amine; 2,5-dibromothiophene-3,4-dicarboxylic acid anhydryde; In tetrahydrofuran; at 50 ℃; for 3h; Inert atmosphere;

With thionyl chloride; In tetrahydrofuran; at 55 ℃; for 4h; Inert atmosphere;
DOI:10.1021/ja400365b