Methyl(2-methyl-1-cyclohexen-1-yl) ketone semicarbazone

Base Information

• Chemical Name: Methyl(2-methyl-1-cyclohexen-1-yl) ketone semicarbazone
• CAS No.: 16983-67-8
• Molecular Formula: C₁₀H₁₇N₃O
• Molecular Weight: 195.264
• Mol file: 16983-67-8.mol

Synonyms:Methyl(2-methyl-1-cyclohexen-1-yl) ketone semicarbazone

Chemical Property of Methyl(2-methyl-1-cyclohexen-1-yl) ketone semicarbazone

Chemical Property:

• Melting Point: 226-227.5 °C
• PKA: 11.98±0.46(Predicted)
• PSA: 67.48000
• Density: 1.17±0.1 g/cm3(Predicted)
• LogP: 3.01230

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Methyl(2-methyl-1-cyclohexen-1-yl) ketone semicarbazone

There total 2 articles about Methyl(2-methyl-1-cyclohexen-1-yl) ketone semicarbazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-methyl-1-acetyl-1-cyclohexene (2047-97-4) → 1-(2-methyl-cyclohex-1-enyl)-ethanone semicarbazone (16983-67-8)

Guidance literature:

DOI:10.1002/hlca.19310140523 DOI:10.1021/ja01135a509 DOI:10.1021/ja01148a003

Reference yield:

1-methylcyclohex-1-ene (591-49-1) → 1-(2-methyl-cyclohex-1-enyl)-ethanone semicarbazone (16983-67-8)

Guidance literature:

Multi-step reaction with 2 steps

1: SnCl₄; carbon disulfide / Erhitzen des Reaktionsprodukts mit N,N-Dimethyl-anilin auf 180grad oder mit N,N-Diaethyl-anilin

With carbon disulfide; tin(IV) chloride;

DOI:10.1002/hlca.19310140523

upstream raw materials:

2-methyl-1-acetyl-1-cyclohexene

1-methylcyclohex-1-ene