Tributylmethylphosphonium Bis(trifluoromethanesulfonyl)imide

Base Information

• Chemical Name: Tributylmethylphosphonium Bis(trifluoromethanesulfonyl)imide
• CAS No.: 324575-10-2
• Molecular Formula: C13H30P.C2F6NO4S2
• Molecular Weight: 497.4971802
• Mol file: 324575-10-2.mol

Synonyms:Tributylmethylphosphonium Bis(trifluoromethanesulfonyl)imide;Tributylmethylphosphonium bis(trifluoromethylsulfonyl)imide

Chemical Property of Tributylmethylphosphonium Bis(trifluoromethanesulfonyl)imide

Chemical Property:

• Melting Point: 16℃
• Refractive Index: 1.4350 to 1.4390
• PSA: 98.63000
• Density: 1.28 g/cm3(Press: 800 Torr)
• LogP: 8.25500

Purity/Quality:

98%,99%, ^*data from raw suppliers

Tributylmethylphosphonium Bis(trifluoromethanesulfonyl)imide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Tributylmethylphosphonium Bis(trifluoromethanesulfonyl)imide

There total 3 articles about Tributylmethylphosphonium Bis(trifluoromethanesulfonyl)imide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

tri-n-butyl(methyl)phosphonium methyl carbonate (120256-45-3) + bis(trifluoromethanesulfonyl)amide (82113-65-3) → tributyl-methyl-phosphonium bis(trifluoromethylsulfonyl)imide (324575-10-2)

Guidance literature:

In methanol; at 20 ℃;

Reference yield:

tributylphosphine (998-40-3) + bis(trifluoromethanesulfonyl)amide (82113-65-3) + carbonic acid dimethyl ester (616-38-6) → tributyl-methyl-phosphonium bis(trifluoromethylsulfonyl)imide (324575-10-2)

Guidance literature:

In methanol; at 0 - 180 ℃; for 7h; under 12001.2 - 12751.3 Torr; Inert atmosphere; Autoclave;

Reference yield:

tributylphosphine (998-40-3) → tributyl-methyl-phosphonium bis(trifluoromethylsulfonyl)imide (324575-10-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 8 h / 145 °C / 10501.1 - 11251.1 Torr

2: methanol / 20 °C

In methanol;

upstream raw materials:

tributylphosphine

bis(trifluoromethanesulfonyl)amide

carbonic acid dimethyl ester

tri-n-butyl(methyl)phosphonium methyl carbonate

Refernces

• 1、 -. "METHOD FOR PREPARING QUATERNARY PHOSPHONIUM SALTS". Paragraph 0032. . Retrieved 2015/06/24.