2-IODOPHENYLHYDRAZINE HYDROCHLORIDE

Base Information

• Chemical Name: 2-IODOPHENYLHYDRAZINE HYDROCHLORIDE
• CAS No.: 60481-34-7
• Molecular Formula: C6H8ClIN2
• Molecular Weight: 270.5
• Mol file: 60481-34-7.mol

Synonyms:2-IODOPHENYLHYDRAZINE HYDROCHLORIDE

Chemical Property of 2-IODOPHENYLHYDRAZINE HYDROCHLORIDE

Chemical Property:

• PSA: 38.05000
• LogP: 3.15210
• Storage Temp.: under inert gas (nitrogen or Argon) at 2–8 °C

Purity/Quality:

97% ^*data from raw suppliers

(2-Iodophenyl)hydrazinehydrochloride 98% ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi

MSDS Files:

Useful:

Technology Process of 2-IODOPHENYLHYDRAZINE HYDROCHLORIDE

There total 2 articles about 2-IODOPHENYLHYDRAZINE HYDROCHLORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

2-iodophenylamine (615-43-0) → (2-iodophenyl)hydrazine hydrochloride (60481-34-7)

Guidance literature:

2-iodophenylamine; With hydrogenchloride; sodium nitrite; In water; at 0 ℃; for 1.5h;

With tin(ll) chloride; In water; at 0 - 20 ℃; for 14.5h;

Reference yield:

→ (2-iodophenyl)hydrazine hydrochloride (60481-34-7)

Guidance literature:

With hydrogenchloride; tin(ll) chloride; sodium nitrite; at 0 - 20 ℃; for 19.5h;

Reference yield: 66.6%

(2-iodophenyl)hydrazine hydrochloride (60481-34-7) + 6,7,8,9-tetrahydro-5H-pyrido[2,3-b]azepine-5,8-dione (652976-28-8) → 5-[2-(2-iodophenyl)hydrazono]-6,7-dihydro-5H-pyrido[2,3-b]azepine-8(9H)-one

Guidance literature:

With sulfuric acid; sodium acetate; In acetic acid; at 20 - 40 ℃; for 9h; Inert atmosphere;

DOI:10.1016/j.ejmech.2014.06.020

upstream raw materials:

2-iodophenylamine

Downstream raw materials:

(1R,2R)-N-(1-cyanocyclopropyl)-2-[(6-cyano-1,3,4,5-tetrahydro-2H-pyrido[4,3-b]indol-2-yl)carbonyl]cyclohexanecarboxamide

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