Technology Process of [2-AMINO-2-(4-METHOXY-PHENYL)-ETHYL]-CARBAMIC ACID TERT-BUTYL ESTER HYDROCHLORIDE
There total 5 articles about [2-AMINO-2-(4-METHOXY-PHENYL)-ETHYL]-CARBAMIC ACID TERT-BUTYL ESTER HYDROCHLORIDE which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium 10% on activated carbon; hydrogen;
In
methanol;
for 5h;
under 2068.65 Torr;
DOI:10.1016/j.bmcl.2016.03.043
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: hexamethylenetetramine; sodium iodide / ethanol / 24 h
1.2: 5 h / Reflux
2.1: sodium hydrogencarbonate / methanol / 12 h
3.1: hydroxylamine hydrochloride; pyridine / ethanol / 3 h
4.1: hydrogen; palladium 10% on activated carbon / methanol / 5 h / 2068.65 Torr
With
pyridine; hexamethylenetetramine; palladium 10% on activated carbon; hydroxylamine hydrochloride; hydrogen; sodium hydrogencarbonate; sodium iodide;
In
methanol; ethanol;
1.1: |Delepine Amine Synthesis / 1.2: |Delepine Amine Synthesis;
DOI:10.1016/j.bmcl.2016.03.043
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium hydrogencarbonate / methanol / 12 h
2: hydroxylamine hydrochloride; pyridine / ethanol / 3 h
3: hydrogen; palladium 10% on activated carbon / methanol / 5 h / 2068.65 Torr
With
pyridine; palladium 10% on activated carbon; hydroxylamine hydrochloride; hydrogen; sodium hydrogencarbonate;
In
methanol; ethanol;
DOI:10.1016/j.bmcl.2016.03.043
