4-(3,3,4,4,5,5,6,6,7,7,8,8,8-Tridecafluorooctyl)benzyl alcohol

Base Information

Chemical Name:4-(3,3,4,4,5,5,6,6,7,7,8,8,8-Tridecafluorooctyl)benzyl alcohol
CAS No.:356055-76-0
Molecular Formula:C15H11F13O
Molecular Weight:454.231
Hs Code.:2906299090
European Community (EC) Number:621-886-0
DSSTox Substance ID:DTXSID90583413
Nikkaji Number:J1.532.767G
Wikidata:Q81986091
Mol file:356055-76-0.mol

Synonyms:356055-76-0;4-(3,3,4,4,5,5,6,6,7,7,8,8,8-Tridecafluorooctyl)benzyl alcohol;4-(1H,1H,2H,2H-Perfluorooctyl)benzyl alcohol;4-((Perfluorohexyl)ethyl)phenylmethanol;[4-(3,3,4,4,5,5,6,6,7,7,8,8,8-Tridecafluorooctyl)phenyl]methanol;(4-(3,3,4,4,5,5,6,6,7,7,8,8,8-Tridecafluorooctyl)phenyl)methanol;SCHEMBL3427358;DTXSID90583413;ZLZILVFJEAYPNQ-UHFFFAOYSA-N;AKOS015888346;NS00018994;4-(3,3,4,4,5,5,6,6,7,7,8,8,8-Tridecafluorooctyl)benzyl alcohol, >=97.0%

Suppliers and Price of 4-(3,3,4,4,5,5,6,6,7,7,8,8,8-Tridecafluorooctyl)benzyl alcohol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
4-(3,3,4,4,5,5,6,6,7,7,8,8,8-Tridecafluorooctyl)benzyl alcohol ≥97.0%
5 g
$ 513.00

Sigma-Aldrich
4-(3,3,4,4,5,5,6,6,7,7,8,8,8-Tridecafluorooctyl)benzyl alcohol ≥97.0%
5g-f
$ 486.00

Sigma-Aldrich
4-(3,3,4,4,5,5,6,6,7,7,8,8,8-Tridecafluorooctyl)benzyl alcohol ≥97.0%
1 g
$ 131.00

Sigma-Aldrich
4-(3,3,4,4,5,5,6,6,7,7,8,8,8-Tridecafluorooctyl)benzyl alcohol ≥97.0%
1g-f
$ 124.00

American Custom Chemicals Corporation
4-(3,3,4,4,5,5,6,6,7,7,8,8,8-TRIDECAFLUOROOCTYL)BENZYL ALCOHOL 95.00%
5G
$ 1249.74

American Custom Chemicals Corporation
4-(3,3,4,4,5,5,6,6,7,7,8,8,8-TRIDECAFLUOROOCTYL)BENZYL ALCOHOL 95.00%
1G
$ 721.71

Total 3 raw suppliers

Chemical Property of 4-(3,3,4,4,5,5,6,6,7,7,8,8,8-Tridecafluorooctyl)benzyl alcohol

Chemical Property:

Vapor Pressure:0.001mmHg at 25°C
Boiling Point:298.215°C at 760 mmHg
Flash Point:134.156°C
PSA：20.23000
Density:1.483g/cm³
LogP:5.85030
XLogP3:6.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:14
Rotatable Bond Count:8
Exact Mass:454.0602311
Heavy Atom Count:29
Complexity:547

Purity/Quality:

98%Min ^*data from raw suppliers

4-(3,3,4,4,5,5,6,6,7,7,8,8,8-Tridecafluorooctyl)benzyl alcohol ≥97.0% ^*data from reagent suppliers

Safty Information:

Pictogram(s): Xi
Hazard Codes:Xi
Statements: 36/37/38-52/53
Safety Statements: 26-61

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC=C1CCC(C(C(C(C(C(F)(F)F)(F)F)(F)F)(F)F)(F)F)(F)F)CO

Technology Process of 4-(3,3,4,4,5,5,6,6,7,7,8,8,8-Tridecafluorooctyl)benzyl alcohol

There total 5 articles about 4-(3,3,4,4,5,5,6,6,7,7,8,8,8-Tridecafluorooctyl)benzyl alcohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 556050-47-6
4-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-octyl)-benzoic acid methyl ester

: 356055-76-0
4-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl)benzyl alcohol

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; at 0 - 5 ℃;
DOI:10.1021/jo0344283

Reference yield:

: 4-(2-perfluorohexyl)ethylbenzaldehyde

: 356055-76-0
4-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl)benzyl alcohol

Guidance literature:: With sodium tetrahydroborate; In ethanol; at 25 ℃; for 16h;
DOI:10.1016/S0040-4020(01)00369-6

Reference yield:

: 2043-57-4,71215-70-8
1,1,1,2,2,3,3,4,4,5,5,6,6-Tridecafluoro-8-iodooctane

: 356055-76-0
4-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl)benzyl alcohol

Guidance literature:: Multi-step reaction with 3 steps

1.1: Zn; 1,2-dibromoethane; TMSCl / tetrahydrofuran / 15 h / 20 °C

1.2: 48 percent / tetrahydrofuran / 12 h / 45 °C

2.1: n-BuLi / hexane; tetrahydrofuran / 0.5 h / -40 °C

3.1: 0.366 g / NaBH₄ / ethanol / 16 h / 25 °C

With sodium tetrahydroborate; n-butyllithium; chloro-trimethyl-silane; ethylene dibromide; zinc; In tetrahydrofuran; ethanol; hexane;
DOI:10.1016/S0040-4020(01)00369-6