2,3,4-TRI-O-ACETYL-BETA-D-RIBOPYRANOSYL BROMIDE

Base Information

• Chemical Name: 2,3,4-TRI-O-ACETYL-BETA-D-RIBOPYRANOSYL BROMIDE
• CAS No.: 3068-30-2
• Molecular Formula: C11H15BrO7
• Molecular Weight: 339.14
• Mol file: 3068-30-2.mol

Synonyms:2,3,4-TRI-O-ACETYL-BETA-D-RIBOPYRANOSYL BROMIDE;BETA-D-RIBOPYRANOSYL BROMIDE TRIACETATE

Chemical Property of 2,3,4-TRI-O-ACETYL-BETA-D-RIBOPYRANOSYL BROMIDE

Chemical Property:

• PSA: 88.13000
• LogP: 0.53270

Purity/Quality:

99% ^*data from raw suppliers

2,3,4-TRI-O-ACETYL-BETA-D-RIBOPYRANOSYL BROMIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,3,4-TRI-O-ACETYL-BETA-D-RIBOPYRANOSYL BROMIDE

There total 6 articles about 2,3,4-TRI-O-ACETYL-BETA-D-RIBOPYRANOSYL BROMIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.2%

1,2,3,4-tetra-O-acetyl-β-D-ribopyranose (4627-30-9) → 2,3,4-tri-O-acetyl-β-D-ribopyranosyl bromide (3068-30-2)

Guidance literature:

With hydrogen bromide; acetic acid; for 2h; Ambient temperature;

DOI:10.1002/(SICI)1099-1344(199707)39:7<541::AID-JLCR5>3.0.CO;2-B

Reference yield:

→ Tri-O-acetyl-β-D-arabinosylbromid (3056-11-9,3068-29-9,3068-30-2,3068-31-3,4049-35-8,4099-16-5,14227-90-8,39524-37-3,39524-39-5,50730-32-0,50837-92-8,51830-02-5,55555-59-4,65914-26-3,75247-31-3,102339-91-3,103530-43-4,113889-50-2,138514-72-4,138514-73-5)

Guidance literature:

Triacetyl-D-arabinose;

Reference yield:

→ Tri-O-acetyl-α-D-xylopyranosylbromid (3056-11-9,3068-29-9,3068-30-2,3068-31-3,4049-35-8,4099-16-5,14227-90-8,39524-37-3,39524-39-5,50730-32-0,50837-92-8,51830-02-5,55555-59-4,65914-26-3,75247-31-3,102339-91-3,103530-43-4,113889-50-2,138514-72-4,138514-73-5)

Guidance literature:

Tetra-O-acetyl-β-D-xylopyranose, gasf. HBr, Eg. (0grad, 2h);

upstream raw materials:

1,2,3,4-tetra-O-acetyl-β-D-ribopyranose

β-D-ribofuranose

acetic anhydride

Downstream raw materials:

3-carbamoyl-1-(tri-O-acetyl-β-D-ribopyranosyl)-pyridinium; bromide

O¹-Phosphono-ξ-D-ribopyranose

Acetic acid (3S,6R)-6-methoxy-3,6-dihydro-2H-pyran-3-yl ester

3,4-di-O-acetyl-D-xylal