1-[1-(2-METHOXYETHYL)PIPERIDIN-4-YL]METHANAMINE

Base Information

• Chemical Name: 1-[1-(2-METHOXYETHYL)PIPERIDIN-4-YL]METHANAMINE
• CAS No.: 956722-57-9
• Molecular Formula: C₉H₂₀N₂O
• Molecular Weight: 172.271
• Hs Code.: 2933399090
• Mol file: 956722-57-9.mol

Synonyms:1-[1-(2-METHOXYETHYL)PIPERIDIN-4-YL]METHANAMINE;UKRORGSYN-BB BBV-105790;1-[1-(2-methoxyethyl)piperidin-4-yl]methanamine(SALTDATA: FREE);C-[1-(2-Methoxy-ethyl)-piperidin-4-yl]-methylamine

Chemical Property of 1-[1-(2-METHOXYETHYL)PIPERIDIN-4-YL]METHANAMINE

Chemical Property:

• Vapor Pressure: 0.0455mmHg at 25°C
• Boiling Point: 237.2°C at 760 mmHg
• Flash Point: 97.2°C
• PSA: 38.49000
• Density: 0.942g/cm³
• LogP: 0.94170

Purity/Quality:

99% ^*data from raw suppliers

[1-(2-methoxyethyl)piperidin-4-yl]methanamine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-[1-(2-METHOXYETHYL)PIPERIDIN-4-YL]METHANAMINE

There total 3 articles about 1-[1-(2-METHOXYETHYL)PIPERIDIN-4-YL]METHANAMINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

N-((1-(2-methoxyethyl)piperidin-4-yl)methyl)-1-phenylmethanimine → 1-[1-(2-methoxyethyl)piperidin-4-yl]methanamine (956722-57-9)

Guidance literature:

With water; oxalic acid; In dichloromethane; for 3h; Reflux;

DOI:10.3390/ph13080161

Reference yield:

4-Aminomethylpiperidine (7144-05-0) → 1-[1-(2-methoxyethyl)piperidin-4-yl]methanamine (956722-57-9)

Guidance literature:

Multi-step reaction with 3 steps

1: ethanol / 24 h / Reflux

2: potassium carbonate / acetone / 12 h / 20 °C

3: oxalic acid; water / dichloromethane / 3 h / Reflux

With water; oxalic acid; potassium carbonate; In ethanol; dichloromethane; acetone;

DOI:10.3390/ph13080161

Reference yield:

N-hexahydro-4-pyridinylmethyl-N-phenylmethylidenamine (71207-29-9) → 1-[1-(2-methoxyethyl)piperidin-4-yl]methanamine (956722-57-9)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / acetone / 12 h / 20 °C

2: oxalic acid; water / dichloromethane / 3 h / Reflux

With water; oxalic acid; potassium carbonate; In dichloromethane; acetone;

DOI:10.3390/ph13080161

upstream raw materials:

4-Aminomethylpiperidine

N-hexahydro-4-pyridinylmethyl-N-phenylmethylidenamine

Downstream raw materials:

C₂₁H₂₅F₃N₆O₂

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