(E)-tert-Butyl 4-(2-ethoxy-2-oxoethylidene)azepane-1-carboxylate

Base Information

• Chemical Name: (E)-tert-Butyl 4-(2-ethoxy-2-oxoethylidene)azepane-1-carboxylate
• CAS No.: 473836-97-4
• Molecular Weight: 283.36
• Mol file: 473836-97-4.mol

Synonyms:(E)-tert-Butyl 4-(2-ethoxy-2-oxoethylidene)azepane-1-carboxylate

Chemical Property of (E)-tert-Butyl 4-(2-ethoxy-2-oxoethylidene)azepane-1-carboxylate

Chemical Property:

• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

99.00% ^*data from raw suppliers

(E)-tert-Butyl4-(2-ethoxy-2-oxoethylidene)azepane-1-carboxylate 95+% ^*data from reagent suppliers

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Technology Process of (E)-tert-Butyl 4-(2-ethoxy-2-oxoethylidene)azepane-1-carboxylate

There total 1 articles about (E)-tert-Butyl 4-(2-ethoxy-2-oxoethylidene)azepane-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tert-butyl 4-oxoazepane-1-carboxylate (188975-88-4) + diethoxyphosphoryl-acetic acid ethyl ester (867-13-0) → (1-tert-butoxycarbonylperhydroazepin-4-ylidene)acetic acid ethyl ester (473836-97-4)

Guidance literature:

diethoxyphosphoryl-acetic acid ethyl ester; With sodium hydride; In tetrahydrofuran; at 0 - 20 ℃; for 1h;

tert-butyl 4-oxoazepane-1-carboxylate; In tetrahydrofuran; at 0 - 20 ℃; for 0.666667h;

upstream raw materials:

tert-butyl 4-oxoazepane-1-carboxylate

diethoxyphosphoryl-acetic acid ethyl ester

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