Octahydro-2-methyl-5-(4-nitrophenyl)pyrrolo[3,4-c]pyrrole

Base Information

Chemical Name:Octahydro-2-methyl-5-(4-nitrophenyl)pyrrolo[3,4-c]pyrrole
CAS No.:1044764-13-7
Molecular Formula:C₁₃H₁₇N₃O₂
Molecular Weight:247.297
Hs Code.:2933990090
Mol file:1044764-13-7.mol

Synonyms:Octahydro-2-methyl-5-(4-nitrophenyl)pyrrolo[3,4-c]pyrrole

Suppliers and Price of Octahydro-2-methyl-5-(4-nitrophenyl)pyrrolo[3,4-c]pyrrole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2-Methyl-5-(4-nitrophenyl)-octahydro-pyrrolo[3,4-c]pyrrole
100mg
$ 330.00

American Custom Chemicals Corporation
2-METHYL-5-(4-NITRO-PHENYL)-OCTAHYDRO-PYRROLO[3,4-C]PYRROLE 95.00%
5MG
$ 499.02

Total 3 raw suppliers

Chemical Property of Octahydro-2-methyl-5-(4-nitrophenyl)pyrrolo[3,4-c]pyrrole

Chemical Property:

PSA：52.30000
Density:1.229
LogP:2.11870

Purity/Quality:

99% ^*data from raw suppliers

2-Methyl-5-(4-nitrophenyl)-octahydro-pyrrolo[3,4-c]pyrrole ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Octahydro-2-methyl-5-(4-nitrophenyl)pyrrolo[3,4-c]pyrrole

There total 3 articles about Octahydro-2-methyl-5-(4-nitrophenyl)pyrrolo[3,4-c]pyrrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 2-methyloctahydropyrrolo[3,4-c]pyrrole 2,2,2-trifluoroacetate

: 350-46-9,178603-76-4
4-Fluoronitrobenzene

: 75-05-8,26809-02-9
acetonitrile

: 1044764-13-7
2-methyl-5-(4-nitrophenyl)octahydropyrrolo[3,4-c]pyrrole

Guidance literature:: With potassium carbonate; for 16h; Reflux;

Reference yield:

: 250275-15-1,1256094-14-0
tert-butyl (3aR,6aS)-hexahydropyrrolo[3,4-c]pyrrole-2(1H)-carboxylate

: 1044764-13-7
2-methyl-5-(4-nitrophenyl)octahydropyrrolo[3,4-c]pyrrole

Guidance literature:: Multi-step reaction with 3 steps

1: sodium tris(acetoxy)borohydride / dichloromethane / 16 h / 20 °C

2: dichloromethane / 0.5 h / 20 °C

3: potassium carbonate / 16 h / Reflux

With sodium tris(acetoxy)borohydride; potassium carbonate; In dichloromethane;

Reference yield:

: 1407156-17-5
5-methylhexahydropyrrolo[3,4-c]pyrrole-2(1H)-carboxylic acid tert-butyl ester

: 1044764-13-7
2-methyl-5-(4-nitrophenyl)octahydropyrrolo[3,4-c]pyrrole

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 0.5 h / 20 °C

2: potassium carbonate / 16 h / Reflux

With potassium carbonate; In dichloromethane;