6-Carboxyisatin methyl es...

Base Information

• Chemical Name: 6-Carboxyisatin methyl es...
• CAS No.: 213670-35-0
• Molecular Formula: C₁₀H₇NO₄
• Molecular Weight: 205.17
• Hs Code.: 2933990090
• Mol file: 213670-35-0.mol

Synonyms:6-Carboxyisatin methyl es...;6-Carboxyisatin Methyl ester;1H-Indole-6-carboxylic acid, 2,3-dihydro-2,3-dioxo-, methyl ester;methyl 2,3-dioxo-2,3-dihydro-1H-indole-6-carboxylate;Methyl 2,3-dioxoindoline-6-carboxylate

Chemical Property of 6-Carboxyisatin methyl es...

Chemical Property:

• PSA: 72.47000
• LogP: 0.74600

Purity/Quality:

99%, ^*data from raw suppliers

6-CarboxyisatinMethylEster ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 6-Carboxyisatin methyl es...

There total 2 articles about 6-Carboxyisatin methyl es... which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

2-oxo-2,3-dihydro-1H-indole-6-carboxylic acid methyl ester (14192-26-8) → methyl 2,3-dioxoindoline-6-carboxylate (213670-35-0)

Guidance literature:

With selenium(IV) oxide; In 1,4-dioxane; at 100 ℃; for 1h;

Reference yield:

C13H13NO5 → methyl 2,3-dioxoindoline-6-carboxylate (213670-35-0)

Guidance literature:

With potassium permanganate; sodium periodate; potassium carbonate; In 1,4-dioxane; tert-butyl alcohol;

DOI:10.1016/j.bmcl.2009.03.043

Reference yield:

methyl 2,3-dioxoindoline-6-carboxylate (213670-35-0) + 2-(bromomethyl)-1-chloro-3-fluorobenzene (68220-26-8) → methyl 1-(2-chloro-6-fluorobenzyl)-2,3-dioxoindoline-6-carboxylate

Guidance literature:

With potassium carbonate; In acetonitrile; at 60 ℃; for 8h;

DOI:10.1016/j.ejmech.2020.112869

upstream raw materials:

2-oxo-2,3-dihydro-1H-indole-6-carboxylic acid methyl ester

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