Carbamic acid, [(1S)-2-amino-1-methyl-2-thioxoethyl]-, 1,1-dimethylethyl ester

Base Information

Chemical Name:Carbamic acid, [(1S)-2-amino-1-methyl-2-thioxoethyl]-, 1,1-dimethylethyl ester
CAS No.:141041-86-3
Molecular Formula:C₈H₁₆N₂O₂S
Molecular Weight:204.293
Hs Code.:
Mol file:141041-86-3.mol

Synonyms:Carbamic acid, [(1S)-2-amino-1-methyl-2-thioxoethyl]-, 1,1-dimethylethyl ester

Suppliers and Price of Carbamic acid, [(1S)-2-amino-1-methyl-2-thioxoethyl]-, 1,1-dimethylethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

AK Scientific
(S)-2-(Tert-Butoxycarbonylamino)propanethioamide
5g
$ 1772.00

Total 3 raw suppliers

Chemical Property of Carbamic acid, [(1S)-2-amino-1-methyl-2-thioxoethyl]-, 1,1-dimethylethyl ester

Chemical Property:

PSA：0.00000
LogP:0.00000

Purity/Quality:

99% ^*data from raw suppliers

(S)-2-(Tert-Butoxycarbonylamino)propanethioamide ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Carbamic acid, [(1S)-2-amino-1-methyl-2-thioxoethyl]-, 1,1-dimethylethyl ester

There total 8 articles about Carbamic acid, [(1S)-2-amino-1-methyl-2-thioxoethyl]-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 78981-25-6,81587-17-9,85642-13-3
tert-butyl (1S)-2-amino-1-methyl-2-oxoethylcarbamate

: 141041-86-3,96929-01-0,140903-30-6
tert-butyl (S)-(1-amino-1-thioxopropan-2-yl)carbamate

Guidance literature:: With Lawessons reagent; In dichloromethane; at 20 ℃; for 16h;

Reference yield:

: 15761-38-3
L-N-Boc-Ala

: 141041-86-3,96929-01-0,140903-30-6
tert-butyl (S)-(1-amino-1-thioxopropan-2-yl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.33 h / 20 °C

1.2: 2 h / 20 °C

2.1: Lawessons reagent / dichloromethane / 12 h / 20 °C

With Lawessons reagent; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1021/jo201675r

Reference yield:

: 28875-17-4
(S)-N-(tert-butoxycarbonyl)alanine methyl ester

: 141041-86-3,96929-01-0,140903-30-6
tert-butyl (S)-(1-amino-1-thioxopropan-2-yl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: ammonia; methanol

2: Lawessons reagent / tetrahydrofuran / 20 °C

With Lawessons reagent; methanol; ammonia; In tetrahydrofuran;